2,4-Quinolinedicarboxylic acid, 6-(phenoxymethyl)-

Base Information

Chemical Name:2,4-Quinolinedicarboxylic acid, 6-(phenoxymethyl)-
CAS No.:927426-26-4
Molecular Formula:C18H13NO5
Molecular Weight:323.305
Hs Code.:

Synonyms:

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Chemical Property of 2,4-Quinolinedicarboxylic acid, 6-(phenoxymethyl)-

Chemical Property:

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Technology Process of 2,4-Quinolinedicarboxylic acid, 6-(phenoxymethyl)-

There total 5 articles about 2,4-Quinolinedicarboxylic acid, 6-(phenoxymethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 927426-24-2
C₂₀H₁₇NO₅

: 927426-26-4
C₁₈H₁₃NO₅

Guidance literature:: C₂₀H₁₇NO₅; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; pH=2;

Reference yield:

: 91493-56-0
6-methylquinoline-2,4-dicarboxylic acid

: 927426-26-4
C₁₈H₁₃NO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / Reflux; Cooling with ice

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux

3.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

3.2: 20 °C

4.1: lithium hydroxide / water; tetrahydrofuran / 20 °C

With N-Bromosuccinimide; thionyl chloride; caesium carbonate; lithium hydroxide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 92200-46-9
2,4-dimethyl 6-methylquinoline-2,4-dicarboxylate

: 927426-26-4
C₁₈H₁₃NO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 20 °C

3.1: lithium hydroxide / water; tetrahydrofuran / 20 °C

With N-Bromosuccinimide; caesium carbonate; lithium hydroxide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide;