15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one

Base Information

Chemical Name:15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one
CAS No.:72041-34-0
Molecular Formula:C₁₈H₁₂O
Molecular Weight:244.293
Hs Code.:
UNII:Y2RMJ3CZ7H
DSSTox Substance ID:DTXSID90222355
Nikkaji Number:J1.271.397E
Wikidata:Q83100560
Mol file:72041-34-0.mol

Synonyms:15,16-dihydro-1,11-methanocyclopenta(a)phenanthren-17-one

Suppliers and Price of 15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
15,16-DIHYDRO-1,11-METHANOCYCLOPENTA(A)PHENANTHREN-17-ONE 95.00%
5MG
$ 504.59

Total 8 raw suppliers

Chemical Property of 15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one

Chemical Property:

Vapor Pressure:5.1E-10mmHg at 25°C
Refractive Index:1.4700 (estimate)
Boiling Point:497.1°C at 760 mmHg
Flash Point:225.2°C
PSA：17.07000
Density:1.381g/cm³
LogP:4.02610
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:244.088815002
Heavy Atom Count:19
Complexity:414

Purity/Quality:

99% ^*data from raw suppliers

15,16-DIHYDRO-1,11-METHANOCYCLOPENTA(A)PHENANTHREN-17-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=O)C2=C1C3=C4C(=C2)CC5=CC=CC(=C54)C=C3

Technology Process of 15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one

There total 4 articles about 15,16-Dihydro-1,11-methanocyclopenta(a)phenanthren-17-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85616-61-1
3-(3,4-dihydro-4,5-methylene-1-phenanthryl)-3-ethoxycarbonylpropionic acid

: 72041-34-0
15,16-dihydro-1,11-methanocyclopenta phenanthren-17-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) zinc chloride, acetic acid, acetic anhydride, 2.) conc. hydrochloric acid / 1.) reflux, 6 h, 2.) water, reflux 2 h

2: 0.64 g / 10percent palladium-on-charcoal / various solvent(s) / 0.5 h / Heating

With hydrogenchloride; acetic anhydride; acetic acid; zinc(II) chloride; palladium on activated charcoal; In various solvent(s);