2-Octen-6-ynoic acid, (2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)-

Base Information

Chemical Name:2-Octen-6-ynoic acid, (2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)-
CAS No.:928112-87-2
Molecular Formula:C₃₁H₃₉NO₆S
Molecular Weight:553.72
Hs Code.:

2-Octen-6-ynoic acid,
(2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy
phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Octen-6-ynoic acid, (2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)-

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Technology Process of 2-Octen-6-ynoic acid, (2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)-

There total 4 articles about 2-Octen-6-ynoic acid, (2R,4R,6R)-6-(4-hexyn-1-yl)tetrahydro-2-methoxy-2-[(4R)-3-[(4-methoxy phenyl)methyl]-2-oxo-4-thiazolidinyl]-2H-pyran-4-yl ester, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 928112-72-5
(Z)-2-octen-6-ynoic acid

: 4-(6-hex-4-ynyl-4-hydroxy-2-methoxy-tetrahydro-pyran-2-yl)-3-(4-methoxy-benzyl)-thiazolidin-2-one

: 928112-87-2
oct-2-en-6-ynoic acid 6-hex-4-ynyl-2-methoxy-2-[3-(4-methoxy-benzyl)-2-oxo-thiazolidin-4-yl]-tetrahydro-pyran-4-yl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In benzene;
DOI:10.1002/chem.200601136

Reference yield:

: 18719-27-2
5-bromo-pent-2-yne

: 928112-87-2
oct-2-en-6-ynoic acid 6-hex-4-ynyl-2-methoxy-2-[3-(4-methoxy-benzyl)-2-oxo-thiazolidin-4-yl]-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium; I₂ / tetrahydrofuran / 1.5 h / Heating

2: 78 percent / Fe(acac)3 / tetrahydrofuran / -30 - 20 °C

3: 74 percent / aq. NaOH / methanol

4: 61 percent / diethyl azodicarboxylate; PPh₃ / benzene

With sodium hydroxide; iodine; magnesium; triphenylphosphine; diethylazodicarboxylate; iron(III)-acetylacetonate; In tetrahydrofuran; methanol; benzene;
DOI:10.1002/chem.200601136

Reference yield:

: 126459-56-1
pent-3-yn-1-ylmagnesium bromide

: 928112-87-2
oct-2-en-6-ynoic acid 6-hex-4-ynyl-2-methoxy-2-[3-(4-methoxy-benzyl)-2-oxo-thiazolidin-4-yl]-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / Fe(acac)3 / tetrahydrofuran / -30 - 20 °C

2: 74 percent / aq. NaOH / methanol

3: 61 percent / diethyl azodicarboxylate; PPh₃ / benzene

With sodium hydroxide; triphenylphosphine; diethylazodicarboxylate; iron(III)-acetylacetonate; In tetrahydrofuran; methanol; benzene;
DOI:10.1002/chem.200601136