Phosphorous acid, 4-[[bis(4-methoxyphenyl)phenylmethyl]thio]butyl bis(2-cyanoethyl) ester

Base Information

Chemical Name:Phosphorous acid, 4-[[bis(4-methoxyphenyl)phenylmethyl]thio]butyl bis(2-cyanoethyl) ester
CAS No.:928625-19-8
Molecular Formula:C31H35N2O5PS
Molecular Weight:578.669
Hs Code.:

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Chemical Property of Phosphorous acid, 4-[[bis(4-methoxyphenyl)phenylmethyl]thio]butyl bis(2-cyanoethyl) ester

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Technology Process of Phosphorous acid, 4-[[bis(4-methoxyphenyl)phenylmethyl]thio]butyl bis(2-cyanoethyl) ester

There total 2 articles about Phosphorous acid, 4-[[bis(4-methoxyphenyl)phenylmethyl]thio]butyl bis(2-cyanoethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 928625-16-5
4-[bis-(4-methoxy-phenyl)-phenyl-methylsulfanyl]-butan-1-ol

: 102690-88-0
bis(2-cyanoethyl) diisopropylamidophosphite

: 928625-19-8
phosphorous acid 4-[bis-(4-methoxy-phenyl)-phenyl-methylsulfanyl]-butyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: With 1H-tetrazole; In acetonitrile; at 25 ℃; for 2h;
DOI:10.1021/jo062087y

Reference yield:

: 928625-17-6
4-[bis-(4-methoxy-phenyl)-phenyl-methylsulfanyl]-butyric acid methyl ester

: 928625-19-8
phosphorous acid 4-[bis-(4-methoxy-phenyl)-phenyl-methylsulfanyl]-butyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

2: 92 percent / 1H-tetrazole / acetonitrile / 2 h / 25 °C

With 1H-tetrazole; lithium aluminium tetrahydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo062087y