Propanoic acid, 2,2-dimethyl-, 4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen yl]methyl]amino]thioxomethyl]amino]butyl ester

Base Information

Chemical Name:Propanoic acid, 2,2-dimethyl-, 4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen yl]methyl]amino]thioxomethyl]amino]butyl ester
CAS No.:928673-58-9
Molecular Formula:C₂₈H₃₉IN₂O₅S
Molecular Weight:642.599
Hs Code.:

Propanoic acid, 2,2-dimethyl-,
4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen
yl]methyl]amino]thioxomethyl]amino]butyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanoic acid, 2,2-dimethyl-, 4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen yl]methyl]amino]thioxomethyl]amino]butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Propanoic acid, 2,2-dimethyl-, 4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen yl]methyl]amino]thioxomethyl]amino]butyl ester

There total 8 articles about Propanoic acid, 2,2-dimethyl-, 4-(3,4-dimethylphenyl)-2-[[[[[2-iodo-5-methoxy-4-(methoxymethoxy)phen yl]methyl]amino]thioxomethyl]amino]butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 926889-00-1
acetic acid 3-methoxy-4-methoxymethoxy-benzyl ester

: 928673-58-9
2,2-dimethyl-propionic acid 4-(3,4-dimethyl-phenyl)-2-[3-(2-iodo-5-methoxy-4-methoxymethoxy-benzyl)-thioureido]-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / CF₃CO₂Ag; I₂ / CH₂Cl₂

2: LiOH / tetrahydrofuran; H₂O

3: DPPA; DBU / toluene

4: PPh₃ / tetrahydrofuran

With lithium hydroxide; diphenyl-phosphinic acid; iodine; silver trifluoroacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2006.09.059

Reference yield:

: (2-iodo-5-methoxy-4-methoxymethoxy-phenyl)-methanol

: 928673-58-9
2,2-dimethyl-propionic acid 4-(3,4-dimethyl-phenyl)-2-[3-(2-iodo-5-methoxy-4-methoxymethoxy-benzyl)-thioureido]-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: DPPA; DBU / toluene

2: PPh₃ / tetrahydrofuran

With diphenyl-phosphinic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmcl.2006.09.059

Reference yield:

: 926889-06-7
1-azidomethyl-2-iodo-5-methoxy-4-methoxymethoxy-benzene

: 928673-58-9
2,2-dimethyl-propionic acid 4-(3,4-dimethyl-phenyl)-2-[3-(2-iodo-5-methoxy-4-methoxymethoxy-benzyl)-thioureido]-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃ / tetrahydrofuran

With triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2006.09.059