7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine

Base Information

Chemical Name:7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine
CAS No.:5241-44-1
Molecular Formula:C12H6ClN5O5
Molecular Weight:335.6595
Hs Code.:
DSSTox Substance ID:DTXSID00385480

Synonyms:7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine;5241-44-1;DTXSID00385480

Suppliers and Price of 7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine

Chemical Property:

Vapor Pressure:4.25E-10mmHg at 25°C
Boiling Point:499.2°Cat760mmHg
Flash Point:255.7°C
Density:1.726g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:2
Exact Mass:335.0057460
Heavy Atom Count:23
Complexity:472

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)[N+](=O)[O-])NC2=C(C3=NON=C3C(=C2)Cl)[N+](=O)[O-]

Technology Process of 7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine

There total 5 articles about 7-chloro-4-nitro-N-(3-nitrophenyl)-2,1,3-benzoxadiazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3482-45-9
2-[(4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-11-hydroxy-4,8,10,14-tetramethyl-3-oxo-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-methyl-heptanoic acid

: 5241-44-1
3-epi-16-Desacetoxy-24,25-dihydro-fusidsaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH, NaHCO₃ / methanol / Heating

2: diethyl ether

3: (i) MeSO₂Cl, Py, CH₂Cl₂, (ii) toluene, collidine

4: (i) H₂, Pd-CaCO₃, aq. EtOH, dioxane, (ii) NaBH₄, MeOH

With sodium hydroxide; sodium hydrogencarbonate; In methanol; diethyl ether;
DOI:10.1016/S0040-4020(01)96970-4

Reference yield:

: C₃₃H₅₂O₇

: 5241-44-1
3-epi-16-Desacetoxy-24,25-dihydro-fusidsaeure-methylester

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl / methanol

2: aq. NaOH, NaHCO₃ / methanol / Heating

3: diethyl ether

4: (i) MeSO₂Cl, Py, CH₂Cl₂, (ii) toluene, collidine

5: (i) H₂, Pd-CaCO₃, aq. EtOH, dioxane, (ii) NaBH₄, MeOH

With hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; In methanol; diethyl ether;
DOI:10.1016/S0040-4020(01)96970-4

Reference yield:

: 5609-66-5
2-[(4S,5S,8S,9S,10S,11R,13R,14S,16R)-11,16-Dihydroxy-4,8,10,14-tetramethyl-3-oxo-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-methyl-heptanoic acid

: 5241-44-1
3-epi-16-Desacetoxy-24,25-dihydro-fusidsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: (i) MeSO₂Cl, Py, CH₂Cl₂, (ii) toluene, collidine

3: (i) H₂, Pd-CaCO₃, aq. EtOH, dioxane, (ii) NaBH₄, MeOH

In diethyl ether;
DOI:10.1016/S0040-4020(01)96970-4