4-(2-methoxyphenyl)-3-methylbut-3-en-2-one

Base Information

Chemical Name:4-(2-methoxyphenyl)-3-methylbut-3-en-2-one
CAS No.:60438-51-9
Molecular Formula:C12H14O2
Molecular Weight:190.242
Hs Code.:

Synonyms:

Suppliers and Price of 4-(2-methoxyphenyl)-3-methylbut-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-(2-methoxyphenyl)-3-methylbut-3-en-2-one

Chemical Property:

Vapor Pressure:0.000549mmHg at 25°C
Boiling Point:311.9°Cat760mmHg
Flash Point:136.7°C
Density:1.031g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(2-methoxyphenyl)-3-methylbut-3-en-2-one

There total 4 articles about 4-(2-methoxyphenyl)-3-methylbut-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1332627-07-2
C₁₂H₁₄O₂

: 60438-51-9
(E)-3-methyl-4-(2-methoxyphenyl)-3-buten-2-one

Guidance literature:: With silver trifluoromethanesulfonate; platinum(II) chloride; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/adsc.201300413

Reference yield: 48.0%

: 135-02-4
ortho-anisaldehyde

: 78-93-3
butanone

: 60438-51-9
(E)-3-methyl-4-(2-methoxyphenyl)-3-buten-2-one

Guidance literature:: With sulfuric acid; acetic acid; for 20h; Ambient temperature;
DOI:10.1246/bcsj.69.2633

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 60438-51-9
(E)-3-methyl-4-(2-methoxyphenyl)-3-buten-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: indium; ammonium chloride / tetrahydrofuran; water / 0 °C

2: platinum(II) chloride; silver trifluoromethanesulfonate / dichloromethane / 5 h / 20 °C / Inert atmosphere

With indium; silver trifluoromethanesulfonate; ammonium chloride; platinum(II) chloride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/adsc.201300413