Benzenebutanoic acid, 2-acetylphenyl ester

Base Information

• Chemical Name: Benzenebutanoic acid, 2-acetylphenyl ester
• CAS No.: 92911-81-4
• Molecular Formula: C₁₈H₁₈O₃
• Molecular Weight: 282.339

Synonyms:

Chemical Property of Benzenebutanoic acid, 2-acetylphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenebutanoic acid, 2-acetylphenyl ester

There total 1 articles about Benzenebutanoic acid, 2-acetylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-hydroxyacetophenone (118-93-4,104809-67-8) + phenylbutyric acid chloride (18496-54-3) → 4-Phenyl-butyric acid 2-acetyl-phenyl ester (92911-81-4)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 48h; Reflux;

Reference yield: 77.0%

4-Phenyl-butyric acid 2-acetyl-phenyl ester (92911-81-4) → 3-methyl-2-(3-phenylpropyl)benzofuran (1388755-26-7)

Guidance literature:

With titanium(III) chloride; zinc; In tetrahydrofuran; Inert atmosphere; Reflux;

Reference yield:

4-Phenyl-butyric acid 2-acetyl-phenyl ester (92911-81-4) → 1-(2-Hydroxy-phenyl)-6-phenyl-hexane-1,3-dione

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; Ambient temperature;

DOI:10.1055/s-1984-31089

upstream raw materials:

o-hydroxyacetophenone

phenylbutyric acid chloride

Downstream raw materials:

2-(3-Phenyl-propyl)-chromen-4-one

3-methyl-2-(3-phenylpropyl)benzofuran

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