L-Tryptophan, N-[[(4-methoxyphenyl)methoxy]carbonyl]-1-[(2,4,6-trimethylphenyl)sulfon yl]-, hydrazide

Base Information

Chemical Name:L-Tryptophan, N-[[(4-methoxyphenyl)methoxy]carbonyl]-1-[(2,4,6-trimethylphenyl)sulfon yl]-, hydrazide
CAS No.:92916-46-6
Molecular Formula:C29H32N4O6S
Molecular Weight:564.662
Hs Code.:

Synonyms:

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Chemical Property of L-Tryptophan, N-[[(4-methoxyphenyl)methoxy]carbonyl]-1-[(2,4,6-trimethylphenyl)sulfon yl]-, hydrazide

Chemical Property:

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Technology Process of L-Tryptophan, N-[[(4-methoxyphenyl)methoxy]carbonyl]-1-[(2,4,6-trimethylphenyl)sulfon yl]-, hydrazide

There total 1 articles about L-Tryptophan, N-[[(4-methoxyphenyl)methoxy]carbonyl]-1-[(2,4,6-trimethylphenyl)sulfon yl]-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 92916-44-4
Z(OMe)-Trp(Mts)-OBzl

: 92916-46-6
Z(OMe)-Trp(Mts)-NHNH₂

Guidance literature:: With hydrazine hydrate; In ethanol; Ambient temperature;
DOI:10.1248/cpb.32.2660

Reference yield:

: 92916-46-6
Z(OMe)-Trp(Mts)-NHNH₂

: Z(OMe)-Trp(Mts)-azide

Guidance literature:: With hydrogenchloride; isopentyl nitrite; In N,N-dimethyl-formamide; for 0.25h;
DOI:10.1248/cpb.32.2660

Reference yield:

: 92916-46-6
Z(OMe)-Trp(Mts)-NHNH₂

: 92916-52-4
H-Trp(Mts)-Met-Asp(OBzl)-Phe-NH₂

Guidance literature:: Multi-step reaction with 3 steps

1: isoamylnitrite, 5.0 N HCl-DMF / dimethylformamide / 0.25 h

2: dimethylformamide / 48 h / 4 °C

3: trifluoroacetic acid, 2percent ethanedithiol in 3,5-dimethylanisole / 1 h

With hydrogenchloride; ethanedithiol in 3,5-dimethylanisole; trifluoroacetic acid; isopentyl nitrite; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.32.2660