Technology Process of 8-Methoxy-12a-methyl-3,4,4a,4b,5,6,10b,11,12,12a-decahydrochrysen-2(1h)-one
There total 55 articles about 8-Methoxy-12a-methyl-3,4,4a,4b,5,6,10b,11,12,12a-decahydrochrysen-2(1h)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
at 20 ℃;
for 24h;
under 15001.2 Torr;
DOI:10.1016/S0039-128X(02)00181-2
- Guidance literature:
-
estrone 3-methyl ether; diazomethyl-trimethyl-silane;
With
scandium tris(trifluoromethanesulfonate);
In
chloroform-d1; hexane;
for 0.25h;
With
tetra-n-butylammoniumfluoride hydrate;
In
tetrahydrofuran; chloroform-d1; hexane;
at 23 ℃;
for 24h;
Inert atmosphere;
With
tetra-n-butylammoniumfluoride hydrate;
In
tetrahydrofuran;
at 23 ℃;
for 0.5h;
Solvent;
Reagent/catalyst;
regioselective reaction;
Inert atmosphere;
DOI:10.3390/molecules22071041
- Guidance literature:
-
With
hydrogenchloride; thiamine diphosphate;
In
ethanol; benzene;
for 72h;
Ambient temperature;
