1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-

Base Information

Chemical Name:1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-
CAS No.:929298-24-8
Molecular Formula:C38H68O4Si3
Molecular Weight:673.212
Hs Code.:

1-Nonanol,
3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil
yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-

Synonyms:

Suppliers and Price of 1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)-

There total 10 articles about 1-Nonanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-9-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-4-methyl-5-[(triethylsilyl)oxy]-, (3S,4S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 929298-35-1
3-(tert-butyl-dimethyl-silanyloxy)-9-(tert-butyl-diphenyl-silanyloxy)-1-(4-isopropyl-2-thioxo-thiazolidin-3-yl)-4-methyl-5-triethylsilanyloxy-nonan-1-one

: 929298-24-8
3-(tert-butyl-dimethyl-silanyloxy)-9-(tert-butyl-diphenyl-silanyloxy)-4-methyl-5-triethylsilanyloxy-nonan-1-ol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; water; at 0 ℃; for 10h;
DOI:10.1021/ol063083i

Reference yield:

: 929298-22-6
7-(tert-butyl-diphenyl-silanyloxy)-2-methyl-3-triethylsilanyloxy-heptanal

: 929298-24-8
3-(tert-butyl-dimethyl-silanyloxy)-9-(tert-butyl-diphenyl-silanyloxy)-4-methyl-5-triethylsilanyloxy-nonan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tin(II) triflate; N-ethylpiperidine / CH₂Cl₂ / 4 h / -40 °C

1.2: 96 percent / CH₂Cl₂ / 1 h / -78 °C

2.1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 6 h / -78 °C

3.1: 78 percent / lithium borohydride / tetrahydrofuran; H₂O / 10 h / 0 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; lithium borohydride; tin(II) trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol063083i

Reference yield:

: 929298-21-5
7-(tert-butyl-diphenyl-silanyloxy)-2-methyl-3-triethylsilanyloxy-heptan-1-ol

: 929298-24-8
3-(tert-butyl-dimethyl-silanyloxy)-9-(tert-butyl-diphenyl-silanyloxy)-4-methyl-5-triethylsilanyloxy-nonan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 70 percent / IBX / CH₂Cl₂; dimethylsulfoxide / 2 h

2.1: tin(II) triflate; N-ethylpiperidine / CH₂Cl₂ / 4 h / -40 °C

2.2: 96 percent / CH₂Cl₂ / 1 h / -78 °C

3.1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 6 h / -78 °C

4.1: 78 percent / lithium borohydride / tetrahydrofuran; H₂O / 10 h / 0 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; lithium borohydride; tin(II) trifluoromethanesulfonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ol063083i