1-chloro-4-(phenylthioMethyl)phthalazine

Base Information

Chemical Name:1-chloro-4-(phenylthioMethyl)phthalazine
CAS No.:929613-64-9
Molecular Formula:C15H11ClN2S
Molecular Weight:286.77900
Hs Code.:
Mol file:929613-64-9.mol

Synonyms:1-Chloro-4-phenylsulfanylmethyl-phthalazine;

Suppliers and Price of 1-chloro-4-(phenylthioMethyl)phthalazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-chloro-4-(phenylthioMethyl)phthalazine

Chemical Property:

Melting Point:151 - 153 °C
PSA：51.08000
LogP:4.57550

Purity/Quality:: 97-99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-chloro-4-(phenylthioMethyl)phthalazine

There total 6 articles about 1-chloro-4-(phenylthioMethyl)phthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 929613-62-7
1-hydroxy-4-phenylthiomethylphthalazine

: 929613-64-9
1-chloro-4-phenylthiomethylphthalazine

Guidance literature:: With pyridine; trichlorophosphate; at 110 ℃; for 1h;
DOI:10.3390/11070574

Reference yield:

: 929613-60-5
methyl 2-(2-(phenylthio)acetyl)benzoate

: 929613-64-9
1-chloro-4-phenylthiomethylphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / hydrazine hydrate / methanol / 5 h / Heating

2: 83 percent / POCl₃; pyridine / 1 h / 110 °C

With pyridine; hydrazine hydrate; trichlorophosphate; In methanol;
DOI:10.3390/11070574

Reference yield:

: 85-44-9
phthalic anhydride

: 929613-64-9
1-chloro-4-phenylthiomethylphthalazine

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / pyridine / 3 h / Heating

2: K₂CO₃ / acetone / 3 h / Heating

3: 80 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 15 h / 20 °C

4: K₂CO₃ / methanol; acetone / 1.5 h / cooling

5: 91 percent / hydrazine hydrate / methanol / 5 h / Heating

6: 83 percent / POCl₃; pyridine / 1 h / 110 °C

With pyridine; phenyltrimethylammonium tribromide; potassium carbonate; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; methanol; acetone;
DOI:10.3390/11070574