3,5-Pyridinedicarboxylic acid, 2-[[2-[[(cyanoamino)(methylthio)methylene]amino]ethoxy]methyl]-4-(2,3- dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Base Information

• Chemical Name: 3,5-Pyridinedicarboxylic acid, 2-[[2-[[(cyanoamino)(methylthio)methylene]amino]ethoxy]methyl]-4-(2,3- dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester
• CAS No.: 93117-89-6
• Molecular Formula: C23H26Cl2N4O5S
• Molecular Weight: 541.455

Synonyms:

Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[[2-[[(cyanoamino)(methylthio)methylene]amino]ethoxy]methyl]-4-(2,3- dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[[2-[[(cyanoamino)(methylthio)methylene]amino]ethoxy]methyl]-4-(2,3- dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

There total 1 articles about 3,5-Pyridinedicarboxylic acid, 2-[[2-[[(cyanoamino)(methylthio)methylene]amino]ethoxy]methyl]-4-(2,3- dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-50-9) + dimethyl N-cyanodithioiminocarbonate (10191-60-3) → N-<2-<<4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridin-2-yl>methoxy>ethyl>-N'-cyano-S-methylisothiourea (93117-89-6)

Guidance literature:

In isopropyl alcohol; Ambient temperature;

DOI:10.1021/jm00123a009

Reference yield: 22.0%

N-<2-<<4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridin-2-yl>methoxy>ethyl>-N'-cyano-S-methylisothiourea (93117-89-6) → 2-<<2-<(5-Amino-1,2,4-oxadiazol-3-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine (118070-86-3)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; for 4h; Heating;

DOI:10.1021/jm00123a009

Reference yield:

N-<2-<<4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridin-2-yl>methoxy>ethyl>-N'-cyano-S-methylisothiourea (93117-89-6) → UK-52831 (93118-77-5)

Guidance literature:

With hydrazine hydrate; In ethanol; Yield given; Heating;

DOI:10.1021/jm00123a009

upstream raw materials:

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

dimethyl N-cyanodithioiminocarbonate

Downstream raw materials:

2-[2-(5-Amino-1-methyl-1H-[1,2,4]triazol-3-ylamino)-ethoxymethyl]-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

2-<<2-<(5-Amino-1,2,4-oxadiazol-3-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine

UK-52831

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