3,5-Pyridinedicarboxylic acid, 2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester
CAS No.:93118-33-3
Molecular Formula:C₂₂H₂₅Cl₂N₅O₆S
Molecular Weight:558.442
Hs Code.:

3,5-Pyridinedicarboxylic acid,
2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2,
3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

There total 2 articles about 3,5-Pyridinedicarboxylic acid, 2-[[2-[(4-amino-1-oxido-1,2,5-thiadiazol-3-yl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 93118-47-9
4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

: 93118-33-3
2-<<2-<(3-Amino-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine

Guidance literature:: With ammonia; for 1h; Ambient temperature;
DOI:10.1021/jm00123a009

Reference yield:

: 88150-50-9
2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

: 93118-33-3
2-<<2-<(3-Amino-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / methanol / 18 h / Heating

2: 49 percent / ethanolic NH₃ / 1 h / Ambient temperature

With ammonia; In methanol;
DOI:10.1021/jm00123a009