Acetic acid, [4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy )methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester

Base Information

Chemical Name:Acetic acid, [4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy )methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester
CAS No.:93134-87-3
Molecular Formula:C26H33Cl2NO8S
Molecular Weight:590.522
Hs Code.:

Acetic acid,
[4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy
)methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester

Synonyms:

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Chemical Property of Acetic acid, [4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy )methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester

Chemical Property:

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Technology Process of Acetic acid, [4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy )methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester

There total 13 articles about Acetic acid, [4-[[3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-4-[(2-methoxyethoxy )methoxy]phenyl]thio]-2,3-dichlorophenoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 93135-28-5
ethyl <2,3-dichloro-<4-hydroxy-3-<(tert-butoxycarbonyl)aminomethyl>phenylthio>phenoxy>acetate

: 93134-87-3
{4-[3-(tert-Butoxycarbonylamino-methyl)-4-(2-methoxy-ethoxymethoxy)-phenylsulfanyl]-2,3-dichloro-phenoxy}-acetic acid ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h;
DOI:10.1021/jm00379a016

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 93134-87-3
{4-[3-(tert-Butoxycarbonylamino-methyl)-4-(2-methoxy-ethoxymethoxy)-phenylsulfanyl]-2,3-dichloro-phenoxy}-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 71 percent / K₂CO₃ / dimethylformamide / Ambient temperature; overnight

2: 95 percent / AlCl₃ / CH₂Cl₂ / Ambient temperature

3: 88 percent / K₂CO₃ / butan-2-one / 2 h / Heating

4: H₂ / 5percent sulfided Pt/C / ethanol

5: 1.) NaNO₂, H₂SO₄, 2.) Na₂SO₄, H₂SO₄ / 1.) H₂O, RT, overnight, 2.) H₂O, reflux, 2 h

6: H₂SO₄ / 2.5 h / Heating

7: H₂SO₄ / acetic acid / Ambient temperature

8: H₂SO₄ / Ambient temperature

9: HCl / ethanol / 4 h / Heating

10: 1.36 g / Et₃N / dimethylformamide / 2.5 h / Ambient temperature

11: 97 percent / diisopropylethylamine / CH₂Cl₂ / 1 h

With hydrogenchloride; aluminium trichloride; sulfuric acid; hydrogen; potassium carbonate; sodium sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium nitrite; sulfided Pt/C; In ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; butanone;
DOI:10.1021/jm00379a016

Reference yield:

: 87181-26-8
2,3-dichloro-4-ethoxybenzenethiol

: 93134-87-3
{4-[3-(tert-Butoxycarbonylamino-methyl)-4-(2-methoxy-ethoxymethoxy)-phenylsulfanyl]-2,3-dichloro-phenoxy}-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 71 percent / K₂CO₃ / dimethylformamide / Ambient temperature; overnight

2: 95 percent / AlCl₃ / CH₂Cl₂ / Ambient temperature

3: 88 percent / K₂CO₃ / butan-2-one / 2 h / Heating

4: H₂ / 5percent sulfided Pt/C / ethanol

5: 1.) NaNO₂, H₂SO₄, 2.) Na₂SO₄, H₂SO₄ / 1.) H₂O, RT, overnight, 2.) H₂O, reflux, 2 h

6: H₂SO₄ / 2.5 h / Heating

7: H₂SO₄ / acetic acid / Ambient temperature

8: H₂SO₄ / Ambient temperature

9: HCl / ethanol / 4 h / Heating

10: 1.36 g / Et₃N / dimethylformamide / 2.5 h / Ambient temperature

11: 97 percent / diisopropylethylamine / CH₂Cl₂ / 1 h

With hydrogenchloride; aluminium trichloride; sulfuric acid; hydrogen; potassium carbonate; sodium sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium nitrite; sulfided Pt/C; In ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; butanone;
DOI:10.1021/jm00379a016