Dipiperidino sulfide

Base Information

• Chemical Name: Dipiperidino sulfide
• CAS No.: 25116-80-7
• Molecular Formula: C10H20 N2 S
• Molecular Weight: 200.348
• Hs Code.: 2933399090
• Mol file: 25116-80-7.mol

Synonyms:Piperidine,1,1'-thiodi- (6CI,7CI,8CI); 1,1'-Thiodipiperidine; Dipiperidino sulfide;N,N'-Thiobis[piperidine]; NSC 203020

Chemical Property of Dipiperidino sulfide

Chemical Property:

• Boiling Point: 294.6°Cat760mmHg
• Flash Point: 132°C
• PSA: 31.78000
• Density: 1.09g/cm³
• LogP: 2.39720

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dipiperidino sulfide

There total 4 articles about Dipiperidino sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

piperidine (110-89-4) → Succinimide (123-56-8,89963-74-6) + N,N'-thiodipiperidine (25116-80-7) + piperidine hydrochloride (6091-44-7)

Guidance literature:

With N-chlorothiophthalimide; In 1,2-dichloro-ethane; at 20 - 25 ℃; for 2h;

Reference yield: 95.0%

piperidine (110-89-4) → benzenesulfonamide (98-10-2) + N,N'-thiodipiperidine (25116-80-7)

Guidance literature:

With N,N'-bis(phenylsulfonyl)sulfoxylic diamide; In 1,2-dichloro-ethane; for 1h; Yields of byproduct given;

Reference yield: 15.0%

1,2-diamino-benzene (95-54-5) → N,N'-thiodipiperidine (25116-80-7) + benzo[1,2,5]thiadiazole (273-13-2,22706-22-5) + 1,3-Dihydro-2,1,3-benzothiadiazole (4377-90-6)

Guidance literature:

With 1-piperidinosulfenyl chloride; In diethyl ether; at -20 ℃;

upstream raw materials:

piperidine

1,2-diamino-benzene

Downstream raw materials:

S-(4-toluenesulfonyl) 4-toluenethiosulfonate

piperidino p-toluenesulfonyl sulfide

bis(piperidinothiocarbonyl)disulfide

bis-(piperidine-1-thiocarbonyl)-hexasulfane

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