1H-Pyrrole-2-propanoic acid, 4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3 -methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester

Base Information

Chemical Name:1H-Pyrrole-2-propanoic acid, 4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3 -methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester
CAS No.:93341-78-7
Molecular Formula:C₃₉H₄₈N₂O₆
Molecular Weight:640.82
Hs Code.:

1H-Pyrrole-2-propanoic acid,
4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3
-methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester

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Chemical Property of 1H-Pyrrole-2-propanoic acid, 4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3 -methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester

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Technology Process of 1H-Pyrrole-2-propanoic acid, 4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3 -methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester

There total 8 articles about 1H-Pyrrole-2-propanoic acid, 4-butyl-b-[4-butyl-3-methyl-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]-3 -methyl-5-[(phenylmethoxy)carbonyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 99851-35-1
diethoxypropionate d'ethyle

: 93341-77-6
benzyloxycarbonyl-2 butyl-3 methyl-4 pyrrol

: C₂₉H₄₄N₂O₆

: 93341-78-7
bis(benzyloxycarbonyl-5, butyl-4, methyl-3, pyrryl-2)-3,3 propionate d'ethyle

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Heating;

Reference yield:

: 34549-87-6
ethyl 4-butyl-3,5-dimethylpyrrole-2-carboxylate

: 93341-78-7
bis(benzyloxycarbonyl-5, butyl-4, methyl-3, pyrryl-2)-3,3 propionate d'ethyle

Guidance literature:: Multi-step reaction with 7 steps

1: 67 percent / sodium / 4 h / 80 °C / 15 Torr

2: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

3: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

4: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

5: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

6: 70 percent / sodium / 4 h / 80 °C / 15 Torr

7: 70 percent / para-toluenesulfonic acid / benzene / 24 h / Heating

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; hydrogen; iodine; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; In tetrahydrofuran; ethanol; water; benzene;

Reference yield:

: 1540-36-9
3-butylpentane-2,4-dione

: 93341-78-7
bis(benzyloxycarbonyl-5, butyl-4, methyl-3, pyrryl-2)-3,3 propionate d'ethyle

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) zinc, sodium acetate / 1.) acetic acid, 80 deg C, 40 min; 2.) acetic acid, 20 min, 95-105 deg C

2: 67 percent / sodium / 4 h / 80 °C / 15 Torr

3: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

4: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

5: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

6: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

7: 70 percent / sodium / 4 h / 80 °C / 15 Torr

8: 70 percent / para-toluenesulfonic acid / benzene / 24 h / Heating

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; hydrogen; iodine; sodium acetate; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; zinc; In tetrahydrofuran; ethanol; water; benzene;