Butanedioic acid, 2,3-bis[(3-hydroxyphenyl)methyl]-, dimethyl ester

Base Information

Chemical Name:Butanedioic acid, 2,3-bis[(3-hydroxyphenyl)methyl]-, dimethyl ester
CAS No.:93578-44-0
Molecular Formula:C20H22O6
Molecular Weight:358.391
Hs Code.:

Synonyms:

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Chemical Property of Butanedioic acid, 2,3-bis[(3-hydroxyphenyl)methyl]-, dimethyl ester

Chemical Property:

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Technology Process of Butanedioic acid, 2,3-bis[(3-hydroxyphenyl)methyl]-, dimethyl ester

There total 5 articles about Butanedioic acid, 2,3-bis[(3-hydroxyphenyl)methyl]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1700-37-4
3-Benzyloxybenzaldehyde

: 93578-44-0
2,3-Bis-(3-hydroxy-benzyl)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethanolate / ethanol / Reflux

2: potassium carbonate / dimethyl sulfoxide / 20 °C

3: sodium ethanolate / ethanol / Reflux

4: potassium carbonate / dimethyl sulfoxide / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethyl [2]alcohol

With palladium 10% on activated carbon; hydrogen; sodium ethanolate; potassium carbonate; In ethanol; ethyl [2]alcohol; dimethyl sulfoxide; 1: |Stobbe Condensation / 3: |Stobbe Condensation;
DOI:10.1016/j.bmc.2015.09.039

Reference yield:

: C₂₀H₂₀O₅

: 93578-44-0
2,3-Bis-(3-hydroxy-benzyl)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: sodium ethanolate / ethanol / Reflux

3: potassium carbonate / dimethyl sulfoxide / 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl [2]alcohol

With palladium 10% on activated carbon; hydrogen; sodium ethanolate; potassium carbonate; In ethanol; ethyl [2]alcohol; dimethyl sulfoxide; 2: |Stobbe Condensation;
DOI:10.1016/j.bmc.2015.09.039

Reference yield:

: C₂₁H₂₂O₅

: 93578-44-0
2,3-Bis-(3-hydroxy-benzyl)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / Reflux

2: potassium carbonate / dimethyl sulfoxide / 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl [2]alcohol

With palladium 10% on activated carbon; hydrogen; sodium ethanolate; potassium carbonate; In ethanol; ethyl [2]alcohol; dimethyl sulfoxide; 1: |Stobbe Condensation;
DOI:10.1016/j.bmc.2015.09.039