Benzenepropanol, a-(4-phenyl-1,3-butadienyl)-

Base Information

Chemical Name:Benzenepropanol, a-(4-phenyl-1,3-butadienyl)-
CAS No.:93604-03-6
Molecular Formula:C19H20O
Molecular Weight:264.367
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanol, a-(4-phenyl-1,3-butadienyl)-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Benzenepropanol, a-(4-phenyl-1,3-butadienyl)-

There total 6 articles about Benzenepropanol, a-(4-phenyl-1,3-butadienyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 38940-11-3
1,7-Diphenyl-1,3-heptadien-5-on

: 93604-03-6
(4E,6E)-1,7-Diphenyl-hepta-4,6-dien-3-ol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; at -30 ℃; for 1h;

Reference yield:

: 72134-60-2
(2-Phenethyl-[1,3]dioxolan-2-yl)-acetaldehyde

: 93604-03-6
(4E,6E)-1,7-Diphenyl-hepta-4,6-dien-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / -15 deg C, 1 h; RT, 2 h

2: lithium aluminum hydride / diethyl ether

3: 78 percent / 46 percent aq. HF / acetonitrile / 0.1 h / Ambient temperature

4: 64 percent / p-toluenesulfonic acid / diethyl ether

5: 89 percent / diisobutylaluminum hydride / diethyl ether / 1 h / -30 °C

With lithium aluminium tetrahydride; hydrogen fluoride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; acetonitrile;

Reference yield:

: 93559-08-1
(2-Phenethyl-[1,3]dioxolan-2-yl)-acetonitrile

: 93604-03-6
(4E,6E)-1,7-Diphenyl-hepta-4,6-dien-3-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 79 percent / diisobutylaluminum hydride / diethyl ether

2: tetrahydrofuran / -15 deg C, 1 h; RT, 2 h

3: lithium aluminum hydride / diethyl ether

4: 78 percent / 46 percent aq. HF / acetonitrile / 0.1 h / Ambient temperature

5: 64 percent / p-toluenesulfonic acid / diethyl ether

6: 89 percent / diisobutylaluminum hydride / diethyl ether / 1 h / -30 °C

With lithium aluminium tetrahydride; hydrogen fluoride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; acetonitrile;