N-Methyl-N-nitroso-p-fluorobenzylamine

Base Information

Chemical Name:N-Methyl-N-nitroso-p-fluorobenzylamine
CAS No.:84174-21-0
Molecular Formula:C8H9FN2O
Molecular Weight:168.171
Hs Code.:2928000090
Mol file:84174-21-0.mol

Synonyms:N-Nitrosomethyl-4-fluorobenzylamine;BENZYLAMINE,p-FLUORO-N-METHYL-N-NITROSO;p-Fluoro-N-methyl-N-nitrosobenzylamine;

Suppliers and Price of N-Methyl-N-nitroso-p-fluorobenzylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-Methyl-N-nitroso-p-fluorobenzylamine

Chemical Property:

Vapor Pressure:0.00161mmHg at 25°C
Boiling Point:304.1°Cat760mmHg
Flash Point:137.7°C
PSA：32.67000
Density:1.13g/cm³
LogP:1.93890

Purity/Quality:: 99%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Methyl-N-nitroso-p-fluorobenzylamine

There total 3 articles about N-Methyl-N-nitroso-p-fluorobenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 405-66-3
(4-Fluoro-benzyl)-methyl-amine

: 84174-21-0
N-(4-fluorobenzyl)-N-methylnitrous amide

Guidance literature:: With potassium nitrite; tetrabutylammonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 4h; Electrochemical reaction;
DOI:10.1002/ejoc.202100363

Reference yield:

: 459-46-1
4-Fluorobenzyl bromide

: 84174-21-0
N-(4-fluorobenzyl)-N-methylnitrous amide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / Heating

2: NaNO₂, aq. HCl / acetic acid; H₂O / Ambient temperature

With hydrogenchloride; sodium nitrite; In ethanol; water; acetic acid;
DOI:10.1021/jm00151a006

Reference yield:

: 84174-25-4
p-fluorobenzylamine formamide

: 84174-21-0
N-(4-fluorobenzyl)-N-methylnitrous amide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / LiAlH₄ / tetrahydrofuran

2: sodium nitrite, aq. acetic acid / 25 h / Ambient temperature

With lithium aluminium tetrahydride; acetic acid; sodium nitrite; In tetrahydrofuran;
DOI:10.1021/jm00357a001