Benzeneacetonitrile, 2,4-dimethoxy-3-methyl-6-(1-methylethoxy)-

Base Information

Chemical Name:Benzeneacetonitrile, 2,4-dimethoxy-3-methyl-6-(1-methylethoxy)-
CAS No.:93681-01-7
Molecular Formula:C14H19NO3
Molecular Weight:249.31
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetonitrile, 2,4-dimethoxy-3-methyl-6-(1-methylethoxy)-

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Technology Process of Benzeneacetonitrile, 2,4-dimethoxy-3-methyl-6-(1-methylethoxy)-

There total 5 articles about Benzeneacetonitrile, 2,4-dimethoxy-3-methyl-6-(1-methylethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 143-33-9,25596-52-5
sodium cyanide

: 93680-99-0
6-isopropoxy-2,4-dimethoxy-3-methylbenzyl chloride

: 93681-01-7
6-isopropoxy-2,4-dimethoxy-3-methylphenylacetonitrile

Guidance literature:: In N,N-dimethyl-formamide; for 20.5h; Ambient temperature;

Reference yield:

: 22080-97-3
3,5-dimethoxy-4-methylphenol

: 93681-01-7
6-isopropoxy-2,4-dimethoxy-3-methylphenylacetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / potassium carbonate / dimethylformamide / 72 h / 50 °C

2: 98 percent / hydrogen chloride (gas) / 1,2-dichloro-ethane / 2 h / 0 °C

3: 98 percent / dimethylformamide / 20.5 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 93681-01-7
6-isopropoxy-2,4-dimethoxy-3-methylphenylacetonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) phosphoryl chloride, 2.) water / 1.) room temperature, 18 h, 2.) 16 h

2: 79 percent / zinc amalgam, hydrochloric acid / acetic acid / 2 h / Heating

3: 81 percent / potassium carbonate / dimethylformamide / 72 h / 50 °C

4: 98 percent / hydrogen chloride (gas) / 1,2-dichloro-ethane / 2 h / 0 °C

5: 98 percent / dimethylformamide / 20.5 h / Ambient temperature

With hydrogenchloride; amalgamated zinc; water; potassium carbonate; trichlorophosphate; In acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;