Benzoic acid, 4-(2-amino-5-methoxy-3-methylphenoxy)-3-bromo-6-methoxy-2-methyl-, methyl ester

Base Information

Chemical Name:Benzoic acid, 4-(2-amino-5-methoxy-3-methylphenoxy)-3-bromo-6-methoxy-2-methyl-, methyl ester
CAS No.:93796-72-6
Molecular Formula:C₁₈H₂₀BrNO₅
Molecular Weight:410.264
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-(2-amino-5-methoxy-3-methylphenoxy)-3-bromo-6-methoxy-2-methyl-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzoic acid, 4-(2-amino-5-methoxy-3-methylphenoxy)-3-bromo-6-methoxy-2-methyl-, methyl ester

There total 9 articles about Benzoic acid, 4-(2-amino-5-methoxy-3-methylphenoxy)-3-bromo-6-methoxy-2-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 93796-66-8
methyl 5-bromo-2-methoxy-4-(5-methoxy-3-methyl-2-nitrophenoxy)-6-methylbenzoate

: 93796-72-6
4-(2-Amino-5-methoxy-3-methyl-phenoxy)-3-bromo-6-methoxy-2-methyl-benzoic acid methyl ester

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In methanol; for 4h; Heating;

Reference yield:

: 58169-99-6
2,3,4,6-tetrabromo-5-methyl-phenol

: 93796-72-6
4-(2-Amino-5-methoxy-3-methyl-phenoxy)-3-bromo-6-methoxy-2-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / aluminium chloride / benzene / 0.5 h / Heating

2: 34 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents

3: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature

4: 75 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C

5: 90 percent / bromine / CH₂Cl₂ / 0.25 h

6: 69 percent / tin(II) chloride dihydrate, hydrochloric acid / methanol / 4 h / Heating

With hydrogenchloride; aluminium trichloride; bromine; nitric acid; potassium carbonate; acetic acid; tin(ll) chloride; copper(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; benzene;

Reference yield:

: 74204-00-5
3-bromo-5-methylphenol

: 93796-72-6
4-(2-Amino-5-methoxy-3-methyl-phenoxy)-3-bromo-6-methoxy-2-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 34 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents

2: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature

3: 75 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C

4: 90 percent / bromine / CH₂Cl₂ / 0.25 h

5: 69 percent / tin(II) chloride dihydrate, hydrochloric acid / methanol / 4 h / Heating

With hydrogenchloride; bromine; nitric acid; potassium carbonate; acetic acid; tin(ll) chloride; copper(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;