3,5-Pyridinedicarboxylic acid, 2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester
CAS No.:93849-08-2
Molecular Formula:C24H29Cl2N3O8
Molecular Weight:558.416
Hs Code.:

3,5-Pyridinedicarboxylic acid,
2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2,
3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Synonyms:

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

There total 2 articles about 3,5-Pyridinedicarboxylic acid, 2-[[2-[(aminocarbonyl)(2-methoxy-2-oxoethyl)amino]ethoxy]methyl]-4-(2, 3-dichlorophenyl)-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 590-28-3
potassium cyanate

: 88150-56-5
methyl 2-<2-<<4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>aminoacetate

: 93849-08-2
1-<2-<<4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>urea

Guidance literature:: With acetic acid; In 1,4-dioxane; water; for 16h; Ambient temperature;
DOI:10.1021/jm00168a041

Reference yield:

: 88150-50-9
2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

: 93849-08-2
1-<2-<<4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>urea

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / K₂CO₃ / acetonitrile / 3 h / Heating

2: 58 percent / AcOH / dioxane; H₂O / 16 h / Ambient temperature

With potassium carbonate; acetic acid; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/jm00168a041