Germolane, 1,1-dimethyl-3,4-diphenyl-, cis-

Base Information

Chemical Name:Germolane, 1,1-dimethyl-3,4-diphenyl-, cis-
CAS No.:94070-43-6
Molecular Formula:C₁₈H₂₂Ge
Molecular Weight:310.963
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germolane, 1,1-dimethyl-3,4-diphenyl-, cis-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Germolane, 1,1-dimethyl-3,4-diphenyl-, cis-

There total 4 articles about Germolane, 1,1-dimethyl-3,4-diphenyl-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94070-48-1
1,1-dimethyl-3,4-diphenyl-1-germacyclopent-3-ene

: 94070-43-6
cis-1,1-dimethyl3,4-diphenylgermacyclopentane

: trans-1,1-dimethyl3,4-diphenylgermacyclopentane

Guidance literature:: With palladium on activated charcoal; hydrogen; In not given; 50 °C, 50 bar; the hydrogenation was very slow; exclusively small amts. of cis/trans mixt. (60/40) produced; identifiedby capillary GLC (quarz column); Kinetics;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 76054-64-3
7,7-dimethyl-1,4,5,6-tetraphenyl-2,3-benzo-7-germanorbornadiene

: 94070-43-6
cis-1,1-dimethyl3,4-diphenylgermacyclopentane

: trans-1,1-dimethyl3,4-diphenylgermacyclopentane

Guidance literature:: In not given; thermolysis at 70°C; 1:1 mixture of products; separation by repeated TLC;
DOI:10.1021/om00110a004

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 135738-42-0
7,7-dimethyl-7-germanorbornadiene

: 94070-43-6
cis-1,1-dimethyl3,4-diphenylgermacyclopentane

: trans-1,1-dimethyl3,4-diphenylgermacyclopentane

Guidance literature:: In benzene; at 70 °C; a 2.5-7 fold molar excess of styrene applied; react. mechanism discussed; isolation and purifn. by crystn. (EtOH), sublimation, or chromy.; 1/1 mixt. of the 2 isomers sepd. by column chromy. (silica gel, hexane); elem. anal.;