1-Phenanthrenecarboxylic acid, 1,2,3,4-tetrahydro-2-(3-methoxyphenyl)-

Base Information

Chemical Name:1-Phenanthrenecarboxylic acid, 1,2,3,4-tetrahydro-2-(3-methoxyphenyl)-
CAS No.:94146-41-5
Molecular Formula:C₂₂H₂₀O₃
Molecular Weight:332.399
Hs Code.:

Synonyms:

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Chemical Property of 1-Phenanthrenecarboxylic acid, 1,2,3,4-tetrahydro-2-(3-methoxyphenyl)-

Chemical Property:

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Technology Process of 1-Phenanthrenecarboxylic acid, 1,2,3,4-tetrahydro-2-(3-methoxyphenyl)-

There total 5 articles about 1-Phenanthrenecarboxylic acid, 1,2,3,4-tetrahydro-2-(3-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2876-70-2
ethyl 2-naphthylacetate

: 94146-41-5
2-(3-methoxyphenyl)-1,2,3,4-tetrahydrophenanthrene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NaOEt / ethanol / Heating

2: 20percent KOH / ethanol / Heating

3: SnCl₄ / 3 h / 120 °C

4: 1) amalgamated zinc / HCl 2) Me₂SO₄ / 1) water, anisole, reflux 2) 2N NaOH, 30 min // comparable yield by heating the keto-acid with N₂H₄*H₂O/KOH in HOCH₂CH₂OH (Wolff-Kishner red.)

With hydrogenchloride; potassium hydroxide; amalgamated zinc; sodium ethanolate; tin(IV) chloride; dimethyl sulfate; In ethanol;

Reference yield:

: 33877-04-2
3-methoxycinnamic acid ethyl ester

: 94146-41-5
2-(3-methoxyphenyl)-1,2,3,4-tetrahydrophenanthrene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NaOEt / ethanol / Heating

2: 20percent KOH / ethanol / Heating

3: SnCl₄ / 3 h / 120 °C

4: 1) amalgamated zinc / HCl 2) Me₂SO₄ / 1) water, anisole, reflux 2) 2N NaOH, 30 min // comparable yield by heating the keto-acid with N₂H₄*H₂O/KOH in HOCH₂CH₂OH (Wolff-Kishner red.)

With hydrogenchloride; potassium hydroxide; amalgamated zinc; sodium ethanolate; tin(IV) chloride; dimethyl sulfate; In ethanol;

Reference yield:

: 94146-68-6
diethyl α-(2-naphthyl)-β-(3-methoxyphenyl)glutarate

: 94146-41-5
2-(3-methoxyphenyl)-1,2,3,4-tetrahydrophenanthrene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 20percent KOH / ethanol / Heating

2: SnCl₄ / 3 h / 120 °C

3: 1) amalgamated zinc / HCl 2) Me₂SO₄ / 1) water, anisole, reflux 2) 2N NaOH, 30 min // comparable yield by heating the keto-acid with N₂H₄*H₂O/KOH in HOCH₂CH₂OH (Wolff-Kishner red.)

With hydrogenchloride; potassium hydroxide; amalgamated zinc; tin(IV) chloride; dimethyl sulfate; In ethanol;