4-Hexenoyl azide, 3,3-dimethyl-6-(phenylmethoxy)-, (E)-

Base Information

Chemical Name:4-Hexenoyl azide, 3,3-dimethyl-6-(phenylmethoxy)-, (E)-
CAS No.:94162-47-7
Molecular Formula:C15H19N3O2
Molecular Weight:273.335
Hs Code.:

Synonyms:

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Chemical Property of 4-Hexenoyl azide, 3,3-dimethyl-6-(phenylmethoxy)-, (E)-

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Technology Process of 4-Hexenoyl azide, 3,3-dimethyl-6-(phenylmethoxy)-, (E)-

There total 6 articles about 4-Hexenoyl azide, 3,3-dimethyl-6-(phenylmethoxy)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86534-20-5
6-(benzyloxy)-3,3-dimethyl-4-hexenoyl chloride

: 94162-47-7
(E)-6-Benzyloxy-3,3-dimethyl-hex-4-enoyl azide

Guidance literature:: With sodium azide; In water; acetone;
DOI:10.1016/S0040-4039(00)87451-1

Reference yield:

: 107-86-8
3,3-dimethyl acrylaldehyde

: 94162-47-7
(E)-6-Benzyloxy-3,3-dimethyl-hex-4-enoyl azide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi / 1.) THF, hexane, -60 deg C, 10 min, 2.) -65 deg C, 30 min

2: propionic acid / 145 - 180 °C

3: 10percent aq. NaOH / 6 h / Heating

4: 71 percent / thionyl chloride / 1 h / Heating

5: NaN₃ / acetone; H₂O / 0.5 h / 0 °C

With sodium hydroxide; n-butyllithium; thionyl chloride; sodium azide; propionic acid; In water; acetone;
DOI:10.1021/jo00202a016

Reference yield:

: 94162-45-5
(E)-6-(benzyloxy)-3,3-dimethyl-4-hexenoic acid

: 94162-47-7
(E)-6-Benzyloxy-3,3-dimethyl-hex-4-enoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / thionyl chloride / 1 h / Heating

2: NaN₃ / acetone; H₂O / 0.5 h / 0 °C

With thionyl chloride; sodium azide; In water; acetone;
DOI:10.1021/jo00202a016