Technology Process of Benzoic acid,
5-[2-[2-iodo-3,5-bis(1-methylethoxy)phenyl]ethenyl]-2,3,4-trimethoxy-,
methyl ester, (E)-
There total 10 articles about Benzoic acid,
5-[2-[2-iodo-3,5-bis(1-methylethoxy)phenyl]ethenyl]-2,3,4-trimethoxy-,
methyl ester, (E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine;
In
toluene;
at 60 ℃;
for 48h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 8.6 g / potassium carbonate, potassium iodide / dimethylformamide / 120 h / 50 °C
2: 7.34 g / lithium aluminium hydride / diethyl ether / 0.25 h / Heating
3: 13.6 g / manganese dioxide / benzene / 5 h / Heating
4: 14.23 g / iodine, silver trifluoroacetate / CHCl3 / 0.25 h
5: 1.034 g / methanol; dimethylformamide / 4.5 h / 90 °C
6: iodine / toluene / 48 h / 60 °C
With
manganese(IV) oxide; lithium aluminium tetrahydride; iodine; silver trifluoroacetate; potassium carbonate; potassium iodide;
In
methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 4.4 g / hydrogen chloride, zinc chloride / 1,2-dichloro-ethane / 1.) 40 deg C, 3.75 h, 2.) 15 h, RT
2: 1.85 g / toluene / 45 h / 60 °C
3: lithium methoxide / methanol; dimethylformamide
4: 1.034 g / methanol; dimethylformamide / 4.5 h / 90 °C
5: iodine / toluene / 48 h / 60 °C
With
hydrogenchloride; lithium methanolate; iodine; zinc(II) chloride;
In
methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
