2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one

Base Information

Chemical Name:2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one
CAS No.:114915-66-1
Molecular Formula:C₁₁H₉N₃O₃
Molecular Weight:231.211
Hs Code.:
DSSTox Substance ID:DTXSID60921545

Synonyms:8-Nitro-4,4a-dihydro-5H-indeno(1,2-c)pyridazin-3-one;114915-66-1;2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one;3H-Indeno(1,2-c)pyridazin-3-one, 2,4,4a,5-tetrahydro-8-nitro-;DTXSID60921545;LS-81904;8-Nitro-4a,5-dihydro-4H-indeno[1,2-c]pyridazin-3-ol

Suppliers and Price of 2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.69g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:231.06439116
Heavy Atom Count:17
Complexity:401

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2CC(=O)NN=C2C3=C1C=CC(=C3)[N+](=O)[O-]

Technology Process of 2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one

There total 4 articles about 2,4,4a,5-Tetrahydro-8-nitro-3H-indeno(1,2-c)pyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: 114915-77-4
6-nitro-2,3-dihydro-1-oxo-2-indene-2-acetic acid

: 114915-66-1
8-nitro-4,4a-dihydro-5H-indeno(1,2-c)pyridazin-3-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;

Reference yield:

: 7103-80-2
(1-oxo-2-indanyl)acetic acid

: 114915-66-1
8-nitro-4,4a-dihydro-5H-indeno(1,2-c)pyridazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / conc. HNO₃ / 2 h / 5 °C

2: 72.6 percent / hydrazine hydrate / ethanol / 3 h / Heating

With nitric acid; hydrazine hydrate; In ethanol;

Reference yield:

: 83-33-0
inden-1-one

: 114915-66-1
8-nitro-4,4a-dihydro-5H-indeno(1,2-c)pyridazin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / NaOH / H₂O; ethanol / 0.25 h / 15 °C

2: 74 percent / Zn dust / acetic acid; H₂O / 0.5 h / 100 °C

3: 48 percent / conc. HNO₃ / 2 h / 5 °C

4: 72.6 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; nitric acid; hydrazine hydrate; zinc; In ethanol; water; acetic acid;