2-Mercapto-5-methoxybenzoic acid

Base Information

Chemical Name:2-Mercapto-5-methoxybenzoic acid
CAS No.:16807-37-7
Molecular Formula:C8H8 O3 S
Molecular Weight:184.216
Hs Code.:2930909090
Mol file:16807-37-7.mol

Synonyms:m-Anisicacid, 6-mercapto- (8CI); 2-Mercapto-5-methoxybenzoic acid;5-Methoxythiosalicylic acid; NSC 372684

Suppliers and Price of 2-Mercapto-5-methoxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Mercapto-5-methoxybenzoicAcid(90%)
250mg
$ 1210.00

American Custom Chemicals Corporation
2-MERCAPTO-5-METHOXYBENZOIC ACID 95.00%
5MG
$ 505.21

AHH
2-mercapto-5-methoxybenzoicacid 97%
1g
$ 155.00

Total 8 raw suppliers

Chemical Property of 2-Mercapto-5-methoxybenzoic acid

Chemical Property:

Vapor Pressure:1.72E-05mmHg at 25°C
Boiling Point:349.8°Cat760mmHg
Flash Point:165.3°C
PSA：85.33000
Density:1.329g/cm³
LogP:1.68210
Storage Temp.:Hygroscopic, Refrigerator, under inert atmosphere
Solubility.:DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

98%min ^*data from raw suppliers

2-Mercapto-5-methoxybenzoicAcid(90%) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses A benzothiophene having antiallergic activity.

Technology Process of 2-Mercapto-5-methoxybenzoic acid

There total 11 articles about 2-Mercapto-5-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

: 104795-62-2
methyl-2-((N,N-dimethylcarbamoyl)thio)-5-methoxybenzoate

: 16807-37-7
5-methoxy-2-sulfanyl-benzoic acid

Guidance literature:: With sodium hydroxide; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/acs.jmedchem.9b00654

Reference yield: 64.0%

: 19532-69-5
2,2'-dithiobis(5-methoxybenzoic acid)

: 16807-37-7
5-methoxy-2-sulfanyl-benzoic acid

Guidance literature:: With acetic acid; zinc; for 4h; Heating;
DOI:10.1021/jm00363a007

Reference yield:

: 2905-82-0
methyl 5-methoxy-2-hydroxybenzoate

: 16807-37-7
5-methoxy-2-sulfanyl-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethylformamide / 20 °C

2: 210 °C

3: aq. NaOH / Heating

With sodium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.55.613