3,4-dihydro-2H-thieno[3,2-b]indole

Base Information

Chemical Name:3,4-dihydro-2H-thieno[3,2-b]indole
CAS No.:94351-00-5
Molecular Formula:C₁₀H₉NS
Molecular Weight:175.254
Hs Code.:
Mol file:94351-00-5.mol

Synonyms:2,3-dihydrothieno[3,2-b]indole;4H-2,3-Dihydrothieno<3,2-b>indol;3,4-Dihydro-2H-thieno[3,2-b]indole;

Suppliers and Price of 3,4-dihydro-2H-thieno[3,2-b]indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 3,4-dihydro-2H-thieno[3,2-b]indole

Chemical Property:

PSA：41.09000
LogP:2.81610

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4-dihydro-2H-thieno[3,2-b]indole

There total 2 articles about 3,4-dihydro-2H-thieno[3,2-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1003-04-9
Tetrahydrothiophen-3-one

: 59-88-1
phenylhydrazine hydrochloride

: 94351-00-5
3,4-dihydro-2H-thieno[3,2-b]indole

Guidance literature:: In ethanol;
DOI:10.1016/j.bmcl.2009.04.029

Reference yield: 48.0%

: 94351-00-5
3,4-dihydro-2H-thieno[3,2-b]indole

Guidance literature:

Reference yield:

: 94351-00-5
3,4-dihydro-2H-thieno[3,2-b]indole

: N-(4-hydroxycarbamoylbenzyl)-2,3-dihydrothieno[3,2-b]indole-1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 2 h / 0 - 20 °C

2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

2.2: 2 h / 80 °C / Inert atmosphere

3.1: potassium hydroxide; hydroxylamine / methanol; tetrahydrofuran; water / 0.17 h / 20 °C

With hydroxylamine; sodium hydride; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c5ob02625c