2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene

Base Information

Chemical Name:2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene
CAS No.:94379-18-7
Molecular Formula:C19H22
Molecular Weight:250.384
Hs Code.:
DSSTox Substance ID:DTXSID301155974
Nikkaji Number:J1.629.264H

Synonyms:2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene;DTXSID301155974;4,6-dimethyl-1-mesitylbenzocyclobutene;94379-18-7

Suppliers and Price of 2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:250.172150702
Heavy Atom Count:19
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)C2CC3=CC(=CC(=C23)C)C)C

Technology Process of 2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene

There total 6 articles about 2,4-Dimethyl-8-(2,4,6-trimethylphenyl)bicyclo[4.2.0]octa-1,3,5-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 61080-14-6
dimesityl diazomethane

: 94379-18-7
2,4-Dimethyl-8-mesityl-bicyclo<4.2.0>octa-1,3,5-trien

Guidance literature:: In benzene; at 140 ℃; Irradiation;
DOI:10.1021/ja00315a014

Reference yield:

: 49633-78-5
2,4,6,2',4',6'-hexamethylbenzophenoneimine

: 94379-18-7
2,4-Dimethyl-8-mesityl-bicyclo<4.2.0>octa-1,3,5-trien

Guidance literature:: Multi-step reaction with 3 steps

1: N₂O₄, sodium acetate / CCl₄ / 1 h / 5 - 10 °C

2: LiAlH₄ / diethyl ether / -30 - -10 °C

3: 70 percent Spectr_. / benzene / 140 °C

With lithium aluminium tetrahydride; sodium acetate; dinitrogen tetraoxide; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1021/ja9635903

Reference yield:

: 409322-39-0
N-Nitroso-dimesityl-ketimin

: 94379-18-7
2,4-Dimethyl-8-mesityl-bicyclo<4.2.0>octa-1,3,5-trien

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / -30 - -10 °C

2: 70 percent Spectr_. / benzene / 140 °C

With lithium aluminium tetrahydride; In diethyl ether; benzene;
DOI:10.1021/ja9635903