Bis(difluorophosphino)methylamine

Base Information

Chemical Name:Bis(difluorophosphino)methylamine
CAS No.:17648-18-9
Molecular Formula:CH₃F₄NP₂
Molecular Weight:166.983
Hs Code.:
DSSTox Substance ID:DTXSID70170143
Nikkaji Number:J1.120.610G
Wikidata:Q83040015
Mol file:17648-18-9.mol

Synonyms:Bis(difluorophosphino)methylamine;17648-18-9;Methyliminobis(difluorophosphine);SCHEMBL6139995;DTXSID70170143

Suppliers and Price of Bis(difluorophosphino)methylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Bis(difluorophosphino)methylamine

Chemical Property:

Vapor Pressure:79.4mmHg at 25°C
Boiling Point:82.2°Cat760mmHg
Flash Point:3.5°C
PSA：30.42000
Density:g/cm³
LogP:3.25000
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:166.96768574
Heavy Atom Count:8
Complexity:59.1

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(P(F)F)P(F)F

Technology Process of Bis(difluorophosphino)methylamine

There total 1 articles about Bis(difluorophosphino)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17648-18-9
bis(difluorophosphino)methylamine

Guidance literature:: MeN(PCl2)2, SbF3;
DOI:10.1039/j19680002689

Reference yield: 95.0%

: 58092-22-1
Co₄(CO)₁₀(μ₄-PPh)₂

: 17648-18-9
bis(difluorophosphino)methylamine

: Co₄(CO)3[(F₂P)2NCH₃]4(P(C₆H₅))2

Guidance literature:: In benzene; heated to ca. 55°C overnight (sealed Pyrex tube); t.l.c. (hexane/benzene, 8/2); isolated; recrystd. (n-hexane, -20°C); elem. anal.;
DOI:10.1039/c39850001102

Reference yield: 85.0%

: Carbonyl(η5-cyclopentadienyl)[bis(dimethylphosphino)methan][1-(4-methylphenyl)-2-oxovinyl]wolfram

: 17648-18-9
bis(difluorophosphino)methylamine

: (η5-Cyclopentadienyl)[1-(4-methylpehnyl)-2-oxovinyl]bis[bis(difluorphosphino)methylamin]wolfram

Guidance literature:: In diethyl ether; byproducts: CO; stirring under at -40°C for 18 h; pptn. with ether and pentane at -78°C, the ppt. decanted, washedwith ether and pentane, dried for 10 h at -30°C in high vac.; elem. anal.;