Cyclohexanone, 3-(bromomethyl)-3-methyl-, (R)-

Base Information

Chemical Name:Cyclohexanone, 3-(bromomethyl)-3-methyl-, (R)-
CAS No.:94390-33-7
Molecular Formula:C8H13BrO
Molecular Weight:205.095
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanone, 3-(bromomethyl)-3-methyl-, (R)-

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Technology Process of Cyclohexanone, 3-(bromomethyl)-3-methyl-, (R)-

There total 1 articles about Cyclohexanone, 3-(bromomethyl)-3-methyl-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 94480-63-4
(1R,6S)-6-Methyl-bicyclo[4.1.0]heptan-2-one

: 94390-33-7
(R)-3-Bromomethyl-3-methyl-cyclohexanone

Guidance literature:: With hydrogen bromide; acetic acid; In benzene; for 0.25h; Ambient temperature;

Reference yield:

: 94390-33-7
(R)-3-Bromomethyl-3-methyl-cyclohexanone

: 94390-35-9
(R)-7-Methyl-7-phenylsulfanylmethyl-1,4-dioxa-spiro[4.5]decane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-TsOH*H₂O / benzene / 0.5 h / Heating

2: 94 percent / aq. 2 N NaOH, hexadecyltributylphosphonium bromide / benzene / 72 h / Heating

With sodium hydroxide; cetyltributylphosphonium bromide; toluene-4-sulfonic acid; In benzene;

Reference yield:

: 94390-33-7
(R)-3-Bromomethyl-3-methyl-cyclohexanone

: 81566-29-2
(R)-7-Benzenesulfonylmethyl-7-methyl-1,4-dioxa-spiro[4.5]decane

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / p-TsOH*H₂O / benzene / 0.5 h / Heating

2: 94 percent / aq. 2 N NaOH, hexadecyltributylphosphonium bromide / benzene / 72 h / Heating

3: 1) aq. 5 percent NaHCO₃, 80 percent m-chloroperbenzoic acid; 2) aq. 10 percent Na₂S₂O₃ / 1) RT, CH₂Cl₂, 1 h

With sodium hydroxide; sodium hydrogencarbonate; cetyltributylphosphonium bromide; toluene-4-sulfonic acid; sodium thiosulfate; 3-chloro-benzenecarboperoxoic acid; In benzene;