2,5-Pyrrolidinedione, 3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl-

Base Information

Chemical Name:2,5-Pyrrolidinedione, 3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl-
CAS No.:94519-11-6
Molecular Formula:C₂₉H₃₄N₄O₂S
Molecular Weight:502.681
Hs Code.:

2,5-Pyrrolidinedione,
3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth
ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Pyrrolidinedione, 3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl-

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Technology Process of 2,5-Pyrrolidinedione, 3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl-

There total 3 articles about 2,5-Pyrrolidinedione, 3-[1-(1,1-dimethylethyl)-5-[(1,1-dimethylethyl)imino]-1,5-dihydro-2-(meth ylthio)-4H-imidazol-4-ylidene]-1-methyl-4,4-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 94519-07-0
N-methyl-3,3-diphenyl-4-cyano-4-(methylthio)succinimide

: 94519-12-7
2-<4-(tert-butylamino)-2-(methylthio)-5-isoimidazol-5-ylidene>-3,3-diphenyl-N-methylsuccinimide

: 94519-11-6
2-<1-tert-butyl-5-(tert-butylimino)-2-(methylthio)-2-imidazol-4-ylidene>-3,3-diphenyl-N-methylsuccinimide

Guidance literature:: In acetonitrile; for 2h; Heating;
DOI:10.1021/jo00206a009

Reference yield: 22.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 94519-08-1
2-cyano-3,3-diphenyl-2-<(tert-butylimino)(methylthio)methyl>-N-methylsuccinimide

: 94519-12-7
2-<4-(tert-butylamino)-2-(methylthio)-5-isoimidazol-5-ylidene>-3,3-diphenyl-N-methylsuccinimide

: 94519-11-6
2-<1-tert-butyl-5-(tert-butylimino)-2-(methylthio)-2-imidazol-4-ylidene>-3,3-diphenyl-N-methylsuccinimide

Guidance literature:: In acetonitrile; for 2h; Heating;
DOI:10.1021/jo00206a009

Reference yield:

: 94519-07-0
N-methyl-3,3-diphenyl-4-cyano-4-(methylthio)succinimide

: 94519-11-6
2-<1-tert-butyl-5-(tert-butylimino)-2-(methylthio)-2-imidazol-4-ylidene>-3,3-diphenyl-N-methylsuccinimide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / CH₂Cl₂ / 15 h / Heating

2: 22 percent / acetonitrile / 2 h / Heating

In dichloromethane; acetonitrile;
DOI:10.1021/jo00206a009