1,3-dimethyl-7-propionyl-2,4(1H,3H)-pteridinedione

Base Information

• Chemical Name: 1,3-dimethyl-7-propionyl-2,4(1H,3H)-pteridinedione
• CAS No.: 94591-39-6
• Molecular Formula: C₁₁H₁₂N₄O₃
• Molecular Weight: 248.241
• Mol file: 94591-39-6.mol

Synonyms:1,3-Dimethyl-7-propionyllumazin;1,3-Dimethyl-7-propionyl-1H-pteridine-2,4-dione;

Chemical Property of 1,3-dimethyl-7-propionyl-2,4(1H,3H)-pteridinedione

Chemical Property:

• Melting Point: 137 - 138 °C
• PSA: 86.85000
• LogP: -0.38010

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1,3-dimethyl-7-propionyl-2,4(1H,3H)-pteridinedione

There total 5 articles about 1,3-dimethyl-7-propionyl-2,4(1H,3H)-pteridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1,3-dimethyllumazine-7-carboxylic acid (71014-19-2) + propionaldehyde (123-38-6) → 1,3-dimethyl-7-propionyllumazine (94591-39-6)

Guidance literature:

With tert.-butylhydroperoxide; iron(II) sulfate; In water; acetic acid; for 0.166667h; Ambient temperature;

Reference yield: 30.0%

1,3-Dimethyllumazine (13401-18-8) + propionaldehyde (123-38-6) → 1,3-dimethyl-7-propionyllumazine (94591-39-6)

Guidance literature:

With tert.-butylhydroperoxide; iron(II) sulfate; In water; acetic acid; for 0.166667h;

Reference yield: 16.0%

1,3-Dimethyllumazine (13401-18-8) + propionaldehyde (123-38-6) → 1,3-Dimethyl-6-propionylpteridine-2,4(1H,3H)-dione (71014-17-0) + 1,3-dimethyl-7-propionyllumazine (94591-39-6)

Guidance literature:

With tert.-butylhydroperoxide; iron(II) sulfate; In trifluoroacetic acid; for 0.25h;

upstream raw materials:

1,3-Dimethyllumazine

propionaldehyde

1,3-dimethyllumazine-7-carboxylic acid

1,3,7-trimethyllumazine

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