3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one

Base Information

• Chemical Name: 3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one
• CAS No.: 94718-41-9
• Molecular Formula: C₁₆H₁₈NO₂P
• Molecular Weight: 287.298
• DSSTox Substance ID: DTXSID10538728

Synonyms:94718-41-9;DTXSID10538728;3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one

Chemical Property of 3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 287.10751581
• Heavy Atom Count: 20
• Complexity: 371

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)C)N2CCOP2(=O)C3=CC=CC=C3

Technology Process of 3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one

There total 1 articles about 3-(2,6-Dimethylphenyl)-2-phenyl-1,3,2lambda~5~-oxazaphospholidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

P,P-dichlorophenylphosphine oxide (824-72-6) + 2-(2,6-dimethylphenylamino)ethanol (3046-95-5) → 2-phenyl-2-oxo-3-(2,6-dimethylphenyl)-1,3,2-oxazaphospholidine (94718-41-9)

Guidance literature:

In pyridine; at 0 - 5 ℃;

DOI:10.1016/S0040-4039(01)91217-1

Reference yield: 5.0%

2-phenyl-2-oxo-3-(2,6-dimethylphenyl)-1,3,2-oxazaphospholidine (94718-41-9) → C16H20NO3P (94718-44-2) + Phenyl-phosphonic acid mono-[2-(2,6-dimethyl-phenylamino)-ethyl] ester (94718-43-1)

Guidance literature:

With water; sodium hydroxide; In 1,4-dioxane; for 0.333333h;

DOI:10.1016/S0040-4039(01)91217-1

upstream raw materials:

P,P-dichlorophenylphosphine oxide

2-(2,6-dimethylphenylamino)ethanol

Downstream raw materials:

C₁₆H₂₀NO₃P

Phenyl-phosphonic acid mono-[2-(2,6-dimethyl-phenylamino)-ethyl] ester

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