(2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol

Base Information

• Chemical Name: (2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol
• CAS No.: 94828-05-4
• Molecular Formula: C23H30O3
• Molecular Weight: 354.489
• Mol file: 94828-05-4.mol

Synonyms:(2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol;8-(1,4-dimethoxy-3-methyl-naphtalen-2-yl)-2,6-dimethyl-octa-2,6-dien-1-ol;

Chemical Property of (2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol

Chemical Property:

• PSA: 38.69000
• LogP: 5.37300

Purity/Quality:

97% ^*data from raw suppliers

(2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol

There total 5 articles about (2E,6E)-8-(1,4-Dimethoxy-3-methylnaphthalen-2-yl)-2,6-dimethylocta-2,6-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2'E)-2-Methyl-3-(3',7'-dimethyl-2',6'-octadienyl)-1,4-dimethoxynaphthalene (53772-25-1) → 8-(1,4-dimethoxy-3-methyl-naphtalen-2-yl)-2,6-dimethyl-octa-2,6-dien-1-ol (94828-05-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 445 mg / SO₂Cl₂ / pyridine; CH₂Cl₂ / 1 h / -20 °C

2: dimethylformamide / 1.) 0 deg C, 1 h; 2.) r.t., 30 min

3: 30percent H₂O₂ / acetic acid / Ambient temperature

4: trimethyl phosphite / methanol / Ambient temperature

With sulfuryl dichloride; dihydrogen peroxide; phosphorous acid trimethyl ester; In pyridine; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;

DOI:10.1248/cpb.32.3952

Reference yield:

2-((E)-6-Benzenesulfinyl-3,7-dimethyl-octa-2,7-dienyl)-1,4-dimethoxy-3-methyl-naphthalene → 8-(1,4-dimethoxy-3-methyl-naphtalen-2-yl)-2,6-dimethyl-octa-2,6-dien-1-ol (94828-05-4)

Guidance literature:

With phosphorous acid trimethyl ester; In methanol; Yield given; Ambient temperature;

DOI:10.1248/cpb.32.3952

Reference yield:

2-((E)-3,7-Dimethyl-6-phenylsulfanyl-octa-2,7-dienyl)-1,4-dimethoxy-3-methyl-naphthalene (94828-25-8) → 8-(1,4-dimethoxy-3-methyl-naphtalen-2-yl)-2,6-dimethyl-octa-2,6-dien-1-ol (94828-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 30percent H₂O₂ / acetic acid / Ambient temperature

2: trimethyl phosphite / methanol / Ambient temperature

With dihydrogen peroxide; phosphorous acid trimethyl ester; In methanol; acetic acid;

DOI:10.1248/cpb.32.3952

upstream raw materials:

(2'E)-2-Methyl-3-(3',7'-dimethyl-2',6'-octadienyl)-1,4-dimethoxynaphthalene

2-((E)-3,7-Dimethyl-6-phenylsulfanyl-octa-2,7-dienyl)-1,4-dimethoxy-3-methyl-naphthalene

2-((E)-6-Chloro-3,7-dimethyl-octa-2,7-dienyl)-1,4-dimethoxy-3-methyl-naphthalene

Downstream raw materials:

menatetrenone

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