o-(3-Nitrophenyl)hydroxylamine

Base Information

Chemical Name:o-(3-Nitrophenyl)hydroxylamine
CAS No.:94831-80-8
Molecular Formula:C6H6N2O3
Molecular Weight:154.125
Hs Code.:
DSSTox Substance ID:DTXSID701306022

Synonyms:o-(3-nitrophenyl)hydroxylamine;94831-80-8;SCHEMBL4766454;DTXSID701306022;AKOS017974744

Suppliers and Price of o-(3-Nitrophenyl)hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-(3-Nitrophenyl)hydroxylamine

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:154.03784206
Heavy Atom Count:11
Complexity:145

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC(=C1)ON)[N+](=O)[O-]

Technology Process of o-(3-Nitrophenyl)hydroxylamine

There total 3 articles about o-(3-Nitrophenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

: N-(3-Nitro-phenoxy)-acetimidic acid ethyl ester

: 94831-80-8
O-(3-nitrophenyl)hydroxylamine

Guidance literature:: With perchloric acid; In 1,4-dioxane; for 1h; Ambient temperature;
DOI:10.1080/00304949709355240

Reference yield:

: 942590-09-2
ethyl (1E)-N-[(3-nitrophenyl)oxy]ethanimidoate

: 94831-80-8
O-(3-nitrophenyl)hydroxylamine

Guidance literature:: ethyl (1E)-N-[(3-nitrophenyl)oxy]ethanimidoate; With perchloric acid; In 1,4-dioxane; water; at 0 ℃; for 2h;

With sodium hydroxide; In 1,4-dioxane; water; pH=> 11;

Reference yield:

: 402-67-5
3-fluoro-1-nitrobenzene

: 94831-80-8
O-(3-nitrophenyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 65.9 percent / t-BuOK / dimethylformamide / 1.) r.t., 30 min, 2.) 80 deg C, 1.5 h

2: 99.9 percent / 70percent aq. HClO₄ / dioxane / 1 h / Ambient temperature

With perchloric acid; potassium tert-butylate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1080/00304949709355240