1,4-Benzenediamine,N1,N4-dibutyl-

Base Information

• Chemical Name: 1,4-Benzenediamine,N1,N4-dibutyl-
• CAS No.: 10368-06-6
• Molecular Formula: C14H24 N2
• Molecular Weight: 220.358
• Mol file: 10368-06-6.mol

Synonyms:1,4-Benzenediamine,N,N'-dibutyl- (9CI); p-Phenylenediamine, N,N'-dibutyl- (6CI,7CI,8CI); Kerobite;N,N'-Dibutyl-p-phenylenediamine

Chemical Property of 1,4-Benzenediamine,N1,N4-dibutyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-Benzenediamine,N1,N4-dibutyl-

There total 7 articles about 1,4-Benzenediamine,N1,N4-dibutyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

n-Butyl chloride (109-69-3) + N,N'-dibenzylidene-benzene-1,4-diamine (797-20-6) → terephthal-bis-butylaniline (10368-06-6)

Guidance literature:

n-Butyl chloride; N,N'-dibenzylidene-benzene-1,4-diamine; In acetonitrile; at 50 ℃; for 5h; under 7500600 Torr;

With hydrogenchloride; In water; for 0.166667h;

DOI:10.1023/A:1022401911074

Reference yield: 72.0%

1,4-phenylenediamine (106-50-3) + butan-1-ol (71-36-3) → terephthal-bis-butylaniline (10368-06-6)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium hydroxide; at 140 ℃; for 48h;

DOI:10.1039/c8cy01200h

Reference yield:

1,4-phenylenediamine (106-50-3) + butan-1-ol (71-36-3) → 2-Ethylhexyl alcohol (104-76-7) + terephthal-bis-butylaniline (10368-06-6)

Guidance literature:

at 220 ℃; unter Druck;

upstream raw materials:

N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine

1,4-phenylenediamine

butan-1-ol

n-Butyl chloride

Downstream raw materials:

N,N'-Dibutyl-N,N'-bis-methylamidosulfonyl-p-phenylendiamin

N,N'-dibutyl-N,N'-p-phenylene-bis-acetamide