2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Base Information

Chemical Name:2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide
CAS No.:5351-82-6
Molecular Formula:C8H8 N4 O3 S
Molecular Weight:240.243
Hs Code.:
Mol file:5351-82-6.mol

Synonyms:Salicylaldehyde, 5-nitro-, thiosemicarbazone(6CI,7CI,8CI); 5-Nitrosalicylaldehyde thiosemicarbazone;NSC 724

Suppliers and Price of 2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Chemical Property:

Vapor Pressure:3.04E-05mmHg at 25°C
Boiling Point:355.8°Cat760mmHg
Flash Point:169°C
Density:1.54g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

There total 4 articles about 2-[(E)-(3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 79-19-6
thiosemicarbazide

: 97-51-8
5-Nitrosalicylaldehyde

: 5351-82-6
1-(2-hydroxy-5-nitrobenzylidene) thiosemicarbazide

Guidance literature:: In ethanol; at 60 - 70 ℃;
DOI:10.1002/hc.10201

Reference yield:

: 79-19-6
thiosemicarbazide

: 97-51-8
5-Nitrosalicylaldehyde

: 5351-82-6
C₈H₈N₄O₃S

Guidance literature:: In ethanol; at 80 ℃; for 2h;
DOI:10.1002/cjoc.201500738

Reference yield:

: C₈H₈N₄O₃S^(2-)*Mg⁽²⁺⁾

: 5351-82-6
1-(2-hydroxy-5-nitrobenzylidene) thiosemicarbazide

Guidance literature:: In ethanol; water; at 25 ℃; Thermodynamic data; Equilibrium constant; μ = 0.1 M,(NaClO4); other temperatures; ΔG(excit), ΔH(excit), ΔS(excit);