Bicyclo[2.2.2]octane-1-carboxaldehyde, 4-phenyl-

Base Information

Chemical Name:Bicyclo[2.2.2]octane-1-carboxaldehyde, 4-phenyl-
CAS No.:94994-29-3
Molecular Formula:C15H18O
Molecular Weight:214.307
Hs Code.:

Synonyms:1-phenylbicyclo[2.2.2]octane-4-carbaldehyde;4-Phenyl-bicyclo[2.2.2]octane-1-carbaldehyde;4-phenylbicyclo[2.2.2]octane-1-carboxaldehyde;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.2]octane-1-carboxaldehyde, 4-phenyl-

Chemical Property:

PSA：17.07000
LogP:3.47750

Purity/Quality:

Safty Information:

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Technology Process of Bicyclo[2.2.2]octane-1-carboxaldehyde, 4-phenyl-

There total 6 articles about Bicyclo[2.2.2]octane-1-carboxaldehyde, 4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 942999-71-5
N-methoxy-N-methyl-1-phenylbicyclo[2.2.2]octane-4-carboxamide

: 94994-29-3
4-phenylbicyclo<2.2.2>octane-1-carboxaldehyde

Guidance literature:: N-methoxy-N-methyl-1-phenylbicyclo[2.2.2]octane-4-carboxamide; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

With water; In tetrahydrofuran;

Reference yield: 86.0%

: 23760-80-7
4-phenylbicyclo<2.2.2>octane-1-methanol

: 94994-29-3
4-phenylbicyclo<2.2.2>octane-1-carboxaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

Reference yield: 83.0%

: 953-69-5
4-phenylbicyclo<2.2.2>octane-1-carboxylic acid

: 94994-29-3
4-phenylbicyclo<2.2.2>octane-1-carboxaldehyde

Guidance literature:: 4-phenylbicyclo<2.2.2>octane-1-carboxylic acid; With 2,6-dimethylpyridine; (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; zinc; dimethyl dicarbonate; In ethyl acetate; for 0.25h; Inert atmosphere; Green chemistry;

With diphenylsilane; In ethyl acetate; at 40 ℃; for 24h; Inert atmosphere; Green chemistry;
DOI:10.1021/acs.orglett.9b02779