2-Bromoacenaphthylen-1(2h)-one

Base Information

Chemical Name:2-Bromoacenaphthylen-1(2h)-one
CAS No.:16269-27-5
Molecular Formula:C12H7 Br O
Molecular Weight:247.091
Hs Code.:
NSC Number:128361
DSSTox Substance ID:DTXSID80299132
Mol file:16269-27-5.mol

Synonyms:16269-27-5;NSC 128361;2-bromoacenaphthylen-1(2h)-one;NSC128361;SCHEMBL7123021;DTXSID80299132;NSC-128361

Suppliers and Price of 2-Bromoacenaphthylen-1(2h)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Bromoacenaphthylen-1(2h)-one

Chemical Property:

Vapor Pressure:1.3E-05mmHg at 25°C
Boiling Point:368.2°Cat760mmHg
Flash Point:129.5°C
Density:1.695g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:245.96803
Heavy Atom Count:14
Complexity:263

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C1)C(C(=O)C3=CC=C2)Br

Technology Process of 2-Bromoacenaphthylen-1(2h)-one

There total 6 articles about 2-Bromoacenaphthylen-1(2h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2235-15-6
1(2H)-acenaphthylenone

: 16269-27-5
2-bromoacenaphthylen-1(2H)-one

Guidance literature:: With copper(ll) bromide; In ethyl acetate; Reflux;
DOI:10.1021/acs.joc.9b03208

Reference yield: 67.0%

: 208-96-8,25036-01-5
acenaphthylene

: 16269-27-5
2-bromoacenaphthylen-1(2H)-one

Guidance literature:: With N-Bromosuccinimide; dimethyl sulfoxide;
DOI:10.1055/s-2002-20473

Reference yield:

: 82-86-0
acenaphthene quinone

: 16269-27-5
2-bromoacenaphthylen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: toluene; PCl₅

2: zinc dust; glacial acetic acid

3: CS₂; bromine

With carbon disulfide; phosphorus pentachloride; bromine; acetic acid; toluene; zinc;