Benzenethiol, 2-amino-4-chloro-, monosodium salt

Base Information

• Chemical Name: Benzenethiol, 2-amino-4-chloro-, monosodium salt
• CAS No.: 95081-18-8
• Molecular Formula: C6H6ClNS.Na
• Molecular Weight: 181.621
• Mol file: 95081-18-8.mol

Synonyms:

Chemical Property of Benzenethiol, 2-amino-4-chloro-, monosodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenethiol, 2-amino-4-chloro-, monosodium salt

There total 2 articles about Benzenethiol, 2-amino-4-chloro-, monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2,5-dichloronitrobenzene (89-61-2) → 2-amino-4-chlorobenzenethiol sodium salt (95081-18-8)

Guidance literature:

With sodium sulfide; In water; for 24h; Heating;

DOI:10.1002/jhet.5570210628

Reference yield:

4-chloro-2-aminobenzenethiol (1004-00-8) → 2-amino-4-chlorobenzenethiol sodium salt (95081-18-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; paraffin oil; at 0 ℃; for 2h;

DOI:10.1016/j.tet.2012.09.010

Reference yield: 85.0%

2-amino-4-chlorobenzenethiol sodium salt (95081-18-8) + p-bromobenzoylacetone → (4-Bromo-phenyl)-(6-chloro-3-methyl-4H-benzo[1,4]thiazin-2-yl)-methanone

Guidance literature:

With hydrogenchloride; In dimethyl sulfoxide; at 40 - 60 ℃; for 0.5h;

upstream raw materials:

2,5-dichloronitrobenzene

4-chloro-2-aminobenzenethiol

Downstream raw materials:

3-(2-Amino-4-chloro-phenylsulfanyl)-thiophene-2-carboxylic acid

6-chloro-3-methyl-2-(p-methylbenzoyl)-4H-1,4-benzothiazine

6-chloro-2-(p-methoxybenzoyl)-3-methyl-4H-1,4-benzothiazine

(R)-5-chloro-2-(1-phenylallylthio)aniline