N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide

Base Information

Chemical Name:N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide
CAS No.:95096-07-4
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:
DSSTox Substance ID:DTXSID801247673

Synonyms:N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide;95096-07-4;DTXSID801247673

Suppliers and Price of N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:209.10519334
Heavy Atom Count:15
Complexity:218

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)N(C(=O)C1=CC=CC=C1OC)O

Technology Process of N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide

There total 1 articles about N-Hydroxy-2-methoxy-N-(1-methylethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5080-22-8
N-isopropylhydroxyamine

: 21615-34-9
2-Methoxybenzoyl chloride

: 95096-07-4
N-Hydroxy-N-isopropyl-2-methoxy-benzamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1055/s-1984-30981

Reference yield:

: 95096-07-4
N-Hydroxy-N-isopropyl-2-methoxy-benzamide

: 95096-09-6
N-Hydroxy-N-isopropyl-2-methoxy-thiobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃, molecular sieves (Linde₄A₁/16'') / CH₂Cl₂ / 6 h

2: Lawesson reagent / CH₂Cl₂ / 6 h / 55 - 60 °C

3: aq. NaOH / tetrahydrofuran / 6 h / 50 °C / pH ca. 8-9

With Lawessons reagent; sodium hydroxide; molecular sieve; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1984-30981

Reference yield:

: 95096-07-4
N-Hydroxy-N-isopropyl-2-methoxy-benzamide

: N-Acetoxy-N-isopropyl-2-methoxy-thiobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃, molecular sieves (Linde₄A₁/16'') / CH₂Cl₂ / 6 h

2: Lawesson reagent / CH₂Cl₂ / 6 h / 55 - 60 °C

With Lawessons reagent; molecular sieve; sodium hydrogencarbonate; In dichloromethane;
DOI:10.1055/s-1984-30981