Plumbane, [(4-chloro-1,3-phenylene)bis(thio)]bis[trimethyl-

Base Information

Chemical Name:Plumbane, [(4-chloro-1,3-phenylene)bis(thio)]bis[trimethyl-
CAS No.:95183-09-8
Molecular Formula:C₁₂H₂₁ClPb₂S₂
Molecular Weight:679.284
Hs Code.:

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Chemical Property of Plumbane, [(4-chloro-1,3-phenylene)bis(thio)]bis[trimethyl-

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Technology Process of Plumbane, [(4-chloro-1,3-phenylene)bis(thio)]bis[trimethyl-

There total 1 articles about Plumbane, [(4-chloro-1,3-phenylene)bis(thio)]bis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3CH₃^(1-)*Pb⁽⁴⁺⁾*CH₃COO^(1-)=(CH₃)3Pb(OOCCH₃)

: 58593-78-5
4-chloro-1,3-benzenedithiol

: 95183-09-8
((CH₃)3Pb)2C₆H₃ClS₂

Guidance literature:: In acetone; exclusion of light; addn. of soln. of dithiol in acetone to a suspension of Pb compd. in acetone (preparing suspension with ice cooling); sepn. of a small amt. of a yellow compd.;; filtration off of ppt. and discarding; concg. the slightly yellow filtrate in vac. at -10°C, sepn. of a slightly yellowish white compd. (quickly turning yellow on exposure to light); elem. anal.;;
DOI:10.1016/0022-328X(84)80542-2