ethyl {1-[1-(hydroxymethyl)propyl]-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl}carbonylcarbamate

Base Information

Chemical Name:ethyl {1-[1-(hydroxymethyl)propyl]-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl}carbonylcarbamate
CAS No.:95337-38-5
Molecular Formula:C₁₂H₁₇N₃O₆
Molecular Weight:299.283
Hs Code.:
Mol file:95337-38-5.mol

Synonyms:[1-(1-Hydroxymethyl-propyl)-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbonyl]-carbamic acid ethyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl {1-[1-(hydroxymethyl)propyl]-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl}carbonylcarbamate

Chemical Property:

Melting Point:228 - 229 °C (methanol)
PSA：130.49000
LogP:-0.24280

Purity/Quality:

Safty Information:

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Technology Process of ethyl {1-[1-(hydroxymethyl)propyl]-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl}carbonylcarbamate

There total 1 articles about ethyl {1-[1-(hydroxymethyl)propyl]-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl}carbonylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 96-20-8,13054-87-0
2-aminobutanol

: 95337-35-2
α-ethoxycarbonylcarbamoyl-β-ethoxy-N-ethoxycarbonylacrylamide

: 95337-38-5
5-ethoxycarbonylcarbamoyl-1-(1-ethyl-2-hydroxyethyl)uracil

Guidance literature:: In water; for 0.166667h;

Reference yield:

: 95337-38-5
5-ethoxycarbonylcarbamoyl-1-(1-ethyl-2-hydroxyethyl)uracil

: 95337-50-1
6-ethoxycarbonylcarbamoyl-3-ethyl-2,3-dihydro-7-oxo-7H-oxazolo<3,2-a>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / Ambient temperature

2: 54 percent / triethylamine / acetone / 2 h / Heating

With triethylamine; In pyridine; acetone;