methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside

Base Information

• Chemical Name: methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside
• CAS No.: 109914-81-0
• Molecular Formula: C₁₅H₂₃NO₁₅S*2Na
• Molecular Weight: 535.391
• Mol file: 109914-81-0.mol

Synonyms:methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside

Chemical Property of methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside

There total 52 articles about methyl 2-acetamido-2-deoxy-3-O-(alpha-idopyranosyluronic acid)-4-O-sulfo-beta-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyl 2-acetamido-6-O-benzyl-2-deoxy-4-O-sulfo-3-O-(2,3,4-tri-O-benzyl-β-L-idopyranosyluronic acid)-β-D-galactopyranoside, disodium salt (109914-80-9,109914-85-4) → methyl 2-acetamido-2-deoxy-3-O-(β-L-idopyranosyluronic acid)-4-O-sulfo-β-D-galactopyranoside, disodium salt (109914-81-0,109914-86-5,128553-04-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; water; for 48h;

DOI:10.1016/S0008-6215(00)90218-0

Reference yield: 86.0%

methyl 2-acetamido-6-O-benzyl-2-deoxy-4-O-sulfo-3-O-(2,3,4-tri-O-benzyl-α-L-idopyranosyluronic acid)-β-D-galactopyranoside, disodium salt (109914-80-9,109914-85-4) → methyl 2-acetamido-2-deoxy-3-O-(α-L-idopyranosyluronic acid)-4-O-sulfo-β-D-galactopyranoside, disodium salt (109914-81-0,109914-86-5,128553-04-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; water; for 36h;

DOI:10.1016/S0008-6215(00)90218-0

Reference yield: 83.0%

methyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-4-O-sulfo-β-D-galactopyranoside, sodium salt (130278-30-7) → methyl 2-acetamido-2-deoxy-3-O-(β-D-glucopyranosyluronic acid)-4-O-sulfo-β-D-galactopyranoside, disodium salt (109914-81-0,109914-86-5,128553-04-8)

Guidance literature:

With sodium hydroxide; In methanol; water; for 6h; Ambient temperature;

DOI:10.1016/0008-6215(90)84259-W

upstream raw materials:

acetic anhydride

methyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-4-O-sulfo-β-D-galactopyranoside, sodium salt

(2R,3R,4R,5R,6R)-5-azido-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4-diol

methyl 2-azido-2-deoxy-4,6-O-benzylidenbe-β-D-galacto-pyranoside