2-(Azidomethyl)-4-chloro-1-nitrobenzene

Base Information

Chemical Name:2-(Azidomethyl)-4-chloro-1-nitrobenzene
CAS No.:95668-82-9
Molecular Formula:C₇H₅ClN₄O₂
Molecular Weight:212.595
Hs Code.:
DSSTox Substance ID:DTXSID80538533
Wikidata:Q82413963

Synonyms:2-(Azidomethyl)-4-chloro-1-nitrobenzene;95668-82-9;DTXSID80538533;AKOS018135894;EN300-279011

Suppliers and Price of 2-(Azidomethyl)-4-chloro-1-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(Azidomethyl)-4-chloro-1-nitrobenzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:212.0101031
Heavy Atom Count:14
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)CN=[N+]=[N-])[N+](=O)[O-]

Technology Process of 2-(Azidomethyl)-4-chloro-1-nitrobenzene

There total 1 articles about 2-(Azidomethyl)-4-chloro-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57750-81-9
4-chloro-2-(chloromethyl)-1-nitrobenzene

: 95668-82-9
5-chloro-2-nitrobenzyl azide

Guidance literature:: With sodium azide; In ethanol; for 6h; Heating;
DOI:10.1002/jhet.5570220221

Reference yield: 51.0%

: 95668-82-9
5-chloro-2-nitrobenzyl azide

: 623-49-4
ethyl cyanoformate

: 95668-83-0
ethyl 1-(5-chloro-2-nitrobenzyl)-5-tetrazolecarboxylate

Guidance literature:: at 145 ℃; for 5h; high pressure;
DOI:10.1002/jhet.5570220221

Reference yield:

: 95668-82-9
5-chloro-2-nitrobenzyl azide

: 95668-84-1
ethyl 1-(2-amino-5-chlorobenzyl)-5-tetrazolecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / 5 h / 145 °C / high pressure

2: 73 percent / Fe powder, HCl gas / ethanol / 1 h

With hydrogenchloride; iron; In ethanol;
DOI:10.1002/jhet.5570220221