1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester
CAS No.:95669-12-8
Molecular Formula:C15H17NO2
Molecular Weight:243.305
Hs Code.:
DSSTox Substance ID:DTXSID40473193
Nikkaji Number:J1.322.637G
Wikidata:Q82302425
Mol file:95669-12-8.mol

Synonyms:1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester;95669-12-8;DTXSID40473193;5-Ethyl-1,2-dihydropyridine-1-carboxylic acid benzyl ester

Suppliers and Price of 1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:243.125928785
Heavy Atom Count:18
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CN(CC=C1)C(=O)OCC2=CC=CC=C2

Technology Process of 1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester

There total 7 articles about 1(2H)-Pyridinecarboxylic acid, 5-ethyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128944-61-6,131454-41-6
1-(benzyloxycarbonyl)-trans-3,4-dibromo-3-ethylpiperidine

: 95669-12-8
1-(benzyloxycarbonyl)-5-ethyl-1,2-dihydropyridine

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In acetonitrile; for 5h; Heating;
DOI:10.1016/S0040-4020(01)81977-3

Reference yield:

: 536-78-7,151103-56-9
3-ethylpyridine

: 95669-12-8
1-(benzyloxycarbonyl)-5-ethyl-1,2-dihydropyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 99.6 percent / 0 - 20 °C

2: NaBH₄ / ethanol / 0 - 20 °C

3: 3.28 g / benzene / 4 h / Heating

4: 98 percent / bromine / CH₂Cl₂

5: DABCO / acetonitrile / 2 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; sodium tetrahydroborate; bromine; In ethanol; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ol990749i

Reference yield:

: 60900-14-3
1-benzyl-3-ethyl-1,2,5,6-tetrahydropyridine

: 95669-12-8
1-(benzyloxycarbonyl)-5-ethyl-1,2-dihydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 3.28 g / benzene / 4 h / Heating

2: 98 percent / bromine / CH₂Cl₂

3: DABCO / acetonitrile / 2 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; bromine; In dichloromethane; acetonitrile; benzene;
DOI:10.1021/ol990749i