Technology Process of Benzaldehyde, 3,6-dimethoxy-2-(1,3,5-undecatrienyl)-, (E,E,E)-
There total 9 articles about Benzaldehyde, 3,6-dimethoxy-2-(1,3,5-undecatrienyl)-, (E,E,E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; dimethyl sulfoxide;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 58.5 percent / anhydrous potassium carbonate / butan-2-one / 192 h / Heating
2: potassium t-butoxide / toluene / 3 h / Heating
3: 84 percent / diethyl ether
4: 82 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 5 h / Heating
5: 82 percent / acetonitrile / 48 h / Ambient temperature
6: 1.) n-butyl-lithium, 3.) iodine
7: 94 percent / lithium aluminium hydride / diethyl ether / 12 h / Ambient temperature
8: 59 percent / oxalyl chloride, dimethyl sulphoxide / CH2Cl2
With
N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; Perbenzoic acid; oxalyl dichloride; potassium tert-butylate; iodine; potassium carbonate; dimethyl sulfoxide;
In
tetrachloromethane; diethyl ether; dichloromethane; toluene; acetonitrile; butanone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 84 percent / diethyl ether
2: 82 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 5 h / Heating
3: 82 percent / acetonitrile / 48 h / Ambient temperature
4: 1.) n-butyl-lithium, 3.) iodine
5: 94 percent / lithium aluminium hydride / diethyl ether / 12 h / Ambient temperature
6: 59 percent / oxalyl chloride, dimethyl sulphoxide / CH2Cl2
With
N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; Perbenzoic acid; oxalyl dichloride; iodine; dimethyl sulfoxide;
In
tetrachloromethane; diethyl ether; dichloromethane; acetonitrile;
